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MassMS-NW-5447 1-fluoronaphthalene C10H7F (Mass of molecular ion: 146)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
50.0 2.3 51.0 1.7 60.0 2.5 62.0 1.3 63.0 2.2 72.0 1.3 73.0 5.7 74.0 2.8 75.0 3.5 94.0 1.7 96.0 1.8 98.0 1.1 99.0 2.4 120.0 6.1 125.0 5.6 126.0 3.8 127.0 1.0 144.0 3.2 145.0 7.2 146.0 100.0 147.0 11.1
90 MHz in CDCl3
400 MHz in CDCl3
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1H NMR 89.56 MHz C10 H7 F 0.04 ml : 0.5 ml CDCl3 1-fluoronaphthalene 
Assign. Shift(ppm)
A 8.08 B 7.80 C 7.55 D *1 7.50 E *1 7.48 G 7.31 J 7.11
Hz ppm Int.729.50 8.146 130 726.75 8.115 126 726.13 8.108 151 724.56 8.091 101 723.88 8.083 100 723.19 8.075 69 722.44 8.067 94 721.50 8.057 73 719.88 8.038 187 706.13 7.885 67 705.75 7.881 70 705.38 7.877 70 705.00 7.872 66 704.00 7.861 76 703.19 7.852 98 701.63 7.835 107 699.50 7.811 167 697.50 7.789 136 696.19 7.774 133 695.81 7.770 127 694.38 7.754 137 692.44 7.732 57 684.31 7.641 115 683.88 7.637 130 683.44 7.632 155 682.44 7.620 128 678.88 7.581 101 678.00 7.571 99 676.19 7.551 276 674.88 7.536 1000 672.06 7.505 302 671.25 7.495 395 668.88 7.469 319 668.06 7.460 410 666.56 7.443 48 665.31 7.429 612 662.56 7.398 229 660.44 7.375 353 655.06 7.315 305 652.38 7.285 197 646.94 7.224 192 645.50 7.208 251 643.94 7.191 242 638.06 7.125 120 636.44 7.107 104 634.88 7.089 235 633.56 7.075 235 627.38 7.006 129 626.06 6.991 122
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1H NMR 399.65 MHz C10 H7 F 0.05 ml : 0.5 ml CDCl3 1-fluoronaphthalene Assign. Shift(ppm)
A 8.09 B 7.80 C 7.564 D *1 7.49 E *1 7.47 G 7.331 J 7.103 J(F-19,G) = 5.4 HZ. J(F-19,J) = 10.7 HZ. J(G,J)= 7.7 HZ. J(C,J)= 1.0 HZ. J(C,G) = 8.3 HZ.
Hz ppm Int.3242.68 8.114 31 3240.36 8.108 71 3237.30 8.101 347 3235.11 8.095 240 3233.03 8.090 305 3227.66 8.077 403 3124.39 7.818 66 3121.95 7.812 230 3120.24 7.808 344 3118.65 7.804 209 3116.70 7.799 255 3115.11 7.795 293 3112.92 7.790 355 3110.72 7.784 275 3107.18 7.775 72 3027.59 7.576 567 3019.29 7.555 678 3010.38 7.533 30 3006.59 7.524 41 3004.52 7.518 40 3000.98 7.510 98 2998.90 7.504 192 2994.14 7.492 626 2992.55 7.488 870 2988.53 7.478 1000 2984.50 7.468 715 2983.03 7.465 677 2978.27 7.453 188 2976.20 7.448 100 2973.39 7.440 33 2973.02 7.440 33 2972.17 7.437 34 2940.31 7.358 325 2934.94 7.344 339 2932.50 7.338 463 2927.12 7.325 461 2924.44 7.318 342 2918.95 7.304 318 2848.02 7.127 369 2847.05 7.124 403 2840.33 7.108 335 2839.36 7.105 363 2837.28 7.100 396 2836.30 7.097 414 2829.59 7.081 317 2828.74 7.079 344
in CDCl3
liquid film
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