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网站主页CAS数据库列表 320339-03-5更多图谱4-叔丁基-4'-碘代联苯(320339-03-5)核磁图(1HNMR)

4-叔丁基-4'-碘代联苯

产品名称 4-叔丁基-4'-碘代联苯

CAS号320339-03-5

分子式C16H17I

分子量336.21

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  • Mass

    MS-KW-0272          
    4-tert-butyl-4'-iodobiphenyl
    C16H17I             (Mass of molecular ion:    336)
    

       Source Temperature: 150 °C
       Sample Temperature: 130 °C
       Direct, 75 eV
    

          29.0       1.5
          39.0       2.3
          41.0       8.0
          50.0       1.1
          51.0       1.8
          55.0       1.0
          57.0       5.5
          63.0       2.2
          69.5       1.3
          70.0       1.0
          74.0       1.0
          75.0       2.0
          76.0       7.4
          77.0       1.6
          81.5       1.4
          82.0      11.2
          82.5       7.3
          83.0      11.8
          83.5       1.7
          88.0       2.5
          89.0       3.4
          94.5       1.1
         102.0       1.0
         104.5       2.2
         115.0       2.3
         117.0       1.1
         126.0       1.2
         127.0       1.2
         139.0       1.4
         146.5      22.5
         147.0       3.3
         150.0       1.6
         151.0       3.6
         152.0       8.9
         153.0       4.9
         154.0       6.6
         160.5       5.9
         165.0      10.1
         166.0       4.5
         167.0       1.2
         176.0       2.1
         177.0       1.9
         178.0       9.0
         179.0       8.3
         180.0       1.4
         191.0       1.2
         193.0       2.6
         194.0      14.5
         195.0       2.6
         293.0      10.0
         294.0       1.5
         321.0     100.0
         322.0      16.5
         323.0       1.3
         336.0      61.0
         337.0      10.7
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C16H17I 0.041 g : 0.5 ml CDCl3
    4-tert-butyl-4'-iodobiphenyl
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.726 B 7.475 C 7.452 D 7.306 E 1.348

         Hz     ppm     Int.
    

       3095.34   7.743     18
       3092.90   7.737    125
       3090.95   7.732     39
       3086.31   7.720     42
       3084.36   7.716    134
       3082.04   7.710     17
       2996.22   7.495     11
       2994.88   7.492     43
       2994.02   7.490     31
       2992.31   7.485     23
       2988.53   7.476     35
       2986.21   7.470    171
       2984.62   7.466     55
       2982.55   7.461     53
       2981.21   7.458    162
       2978.64   7.451     28
       2974.98   7.442     19
       2973.27   7.438     28
       2972.42   7.436     39
       2927.13   7.322     21
       2924.81   7.316    137
       2922.86   7.312     41
       2918.22   7.300     40
       2916.26   7.295    120
       2913.82   7.289     14
        538.95   1.349   1000
    

KBr disk



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