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MassMS-IW-0565 1-phenyl-1-cyclopropanemethanol C10H12O (Mass of molecular ion: 148)
Source Temperature: 260 °C Sample Temperature: 130 °C Reservoir, 75 eV
18.0 1.2 27.0 5.0 28.0 1.3 29.0 1.5 31.0 3.8 38.0 1.0 39.0 15.0 40.0 1.5 41.0 6.7 42.0 1.2 43.0 4.3 50.0 4.6 51.0 16.6 52.0 4.1 53.0 2.5 55.0 8.5 57.0 1.8 62.0 2.1 63.0 8.9 64.0 5.3 65.0 15.0 66.0 1.7 69.0 2.8 70.0 1.3 74.0 1.8 75.0 2.7 76.0 3.5 77.0 18.6 78.0 17.5 79.0 7.5 89.0 7.4 90.0 2.4 91.0 89.1 92.0 14.9 93.0 1.0 102.0 6.7 103.0 9.3 104.0 8.5 105.0 22.0 106.0 8.3 107.0 1.7 115.0 64.0 116.0 14.6 117.0 100.0 118.0 43.0 119.0 9.4 120.0 25.3 121.0 2.2 127.0 3.3 128.0 7.5 129.0 18.5 130.0 36.5 131.0 5.8 133.0 20.1 134.0 2.0 147.0 6.4 148.0 32.2 149.0 3.5
400 MHz in CDCl3
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1H NMR 399.65 MHz C10 H12 O 0.039 g : 0.5 ml CDCl3 1-phenyl-1-cyclopropanemethanol 
Assign. Shift(ppm)
A 7.344 B 7.300 C 7.211 D 3.628 E 1.65 F *1 0.863 G *1 0.830
Hz ppm Int.2941.77 7.361 427 2940.19 7.357 568 2938.11 7.352 207 2935.30 7.345 285 2934.20 7.342 483 2933.35 7.340 993 2932.01 7.337 883 2930.18 7.332 215 2924.56 7.318 475 2923.95 7.317 710 2922.00 7.312 213 2920.17 7.307 64 2918.58 7.303 230 2917.48 7.301 622 2916.75 7.299 1000 2915.16 7.295 396 2910.64 7.283 243 2908.94 7.279 414 2907.10 7.275 95 2889.40 7.230 235 2887.82 7.226 447 2886.23 7.222 244 2884.28 7.218 38 2882.93 7.214 184 2880.62 7.208 411 2878.42 7.203 148 2875.00 7.194 118 2873.54 7.191 201 2872.07 7.187 109 1450.20 3.629 905 659.79 1.651 249 354.86 0.888 61 352.66 0.883 172 350.59 0.878 34 345.95 0.866 741 345.09 0.864 759 343.02 0.859 578 342.04 0.856 662 334.47 0.837 716 333.50 0.835 709 332.28 0.832 688 331.67 0.830 771 330.81 0.828 773 330.32 0.827 743 323.97 0.811 194 321.90 0.806 67
in CDCl3
KBr disc
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