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网站主页CAS数据库列表 3088-41-3更多图谱N-氰乙基哌啶(3088-41-3)核磁图(1HNMR)

N-氰乙基哌啶

产品名称 N-氰乙基哌啶

CAS号3088-41-3

分子式C8H14N2

分子量138.21

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  • Mass

    MS-NW-7604          
    1-piperidinepropionitrile
    C8H14N2             (Mass of molecular ion:    138)
    

       Source Temperature: 250 °C
       Sample Temperature: 170 °C
       Reservoir, 75 eV
    

          15.0       1.8
          18.0       1.1
          26.0       3.8
          27.0       6.4
          28.0       7.0
          29.0       3.7
          30.0       3.8
          39.0       4.9
          40.0       2.0
          41.0      16.2
          42.0      21.4
          43.0       3.0
          44.0       7.1
          51.0       1.9
          52.0       4.4
          53.0       5.0
          54.0       7.3
          55.0      14.6
          56.0       4.5
          57.0       2.7
          67.0       1.3
          68.0       1.8
          69.0       5.1
          70.0       4.4
          79.0       1.7
          81.0       1.3
          82.0       1.8
          83.0       2.8
          84.0       4.7
          85.0       2.0
          96.0       4.6
          97.0       2.2
          98.0     100.0
          99.0       7.1
         109.0       1.0
         137.0       3.0
         138.0       2.8
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C8 H14 N2 0.05 ml : 0.5 ml CDCl3
    1-piperidinepropionitrile
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.660 B 2.504 C 2.428 D 1.582 E 1.433

         Hz     ppm     Int.
    

       1071.17   2.681    432
       1070.31   2.679    460
       1067.50   2.672     89
       1063.23   2.661   1000
       1058.84   2.650     92
       1056.76   2.645    665
       1056.15   2.643    711
       1017.70   2.547     30
       1007.93   2.523    697
       1007.32   2.521    719
       1000.98   2.505    985
       1000.24   2.503    861
        996.70   2.494     94
        993.77   2.487    465
        993.04   2.485    480
        988.77   2.475     62
        987.79   2.472     62
        975.71   2.442    518
        970.58   2.429    694
        965.33   2.416    550
        643.92   1.612    274
        638.06   1.597    532
        632.32   1.583    787
        626.71   1.569    674
        621.34   1.555    356
        583.86   1.461    160
        577.88   1.446    300
        572.27   1.432    369
        566.41   1.418    209
        561.04   1.404     86
    

in CDCl3



liquid film