-
MS-NW-7604 1-piperidinepropionitrile C8H14N2 (Mass of molecular ion: 138)
Source Temperature: 250 °C Sample Temperature: 170 °C Reservoir, 75 eV
15.0 1.8 18.0 1.1 26.0 3.8 27.0 6.4 28.0 7.0 29.0 3.7 30.0 3.8 39.0 4.9 40.0 2.0 41.0 16.2 42.0 21.4 43.0 3.0 44.0 7.1 51.0 1.9 52.0 4.4 53.0 5.0 54.0 7.3 55.0 14.6 56.0 4.5 57.0 2.7 67.0 1.3 68.0 1.8 69.0 5.1 70.0 4.4 79.0 1.7 81.0 1.3 82.0 1.8 83.0 2.8 84.0 4.7 85.0 2.0 96.0 4.6 97.0 2.2 98.0 100.0 99.0 7.1 109.0 1.0 137.0 3.0 138.0 2.8
400 MHz in CDCl3
-
1H NMR 399.65 MHz C8 H14 N2 0.05 ml : 0.5 ml CDCl3 1-piperidinepropionitrile Assign. Shift(ppm)
A 2.660 B 2.504 C 2.428 D 1.582 E 1.433
Hz ppm Int.
1071.17 2.681 432 1070.31 2.679 460 1067.50 2.672 89 1063.23 2.661 1000 1058.84 2.650 92 1056.76 2.645 665 1056.15 2.643 711 1017.70 2.547 30 1007.93 2.523 697 1007.32 2.521 719 1000.98 2.505 985 1000.24 2.503 861 996.70 2.494 94 993.77 2.487 465 993.04 2.485 480 988.77 2.475 62 987.79 2.472 62 975.71 2.442 518 970.58 2.429 694 965.33 2.416 550 643.92 1.612 274 638.06 1.597 532 632.32 1.583 787 626.71 1.569 674 621.34 1.555 356 583.86 1.461 160 577.88 1.446 300 572.27 1.432 369 566.41 1.418 209 561.04 1.404 86
更多供应商