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MassMS-NW-6434 endo-3-chloro-2-norbornanone C7H9ClO (Mass of molecular ion: 144)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
18.0 1.1 26.0 3.3 27.0 16.0 28.0 1.3 29.0 1.4 36.0 1.6 37.0 1.2 38.0 3.2 39.0 22.0 40.0 4.4 41.0 26.2 42.0 1.4 49.0 1.9 50.0 3.4 51.0 6.5 52.0 3.6 53.0 14.6 54.0 15.7 55.0 5.6 63.0 1.1 65.0 4.3 66.0 9.8 67.0 100.0 68.0 7.3 69.0 1.0 75.0 45.9 76.0 2.4 77.0 15.4 78.0 1.3 79.0 13.3 80.0 25.0 81.0 81.9 82.0 5.7 88.0 7.4 90.0 2.3 101.0 1.0 109.0 7.0 115.0 1.7 144.0 31.5 145.0 2.5 146.0 10.6
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H9 Cl O 0.05 ml : 0.5 ml CDCl3 endo-3-chloro-2-norbornanone 
Assign. Shift(ppm)
A 3.693 B 2.72 C 2.242 D *1 1.961 E *2 1.864 F 1.622 G *2 1.556 J *1 1.509 ASSIGNED BY C-H COSY
Hz ppm Int.1477.54 3.698 941 1474.49 3.690 1000 1092.16 2.733 455 1089.11 2.726 441 1087.16 2.721 678 1085.82 2.717 780 1084.59 2.714 594 1082.89 2.710 411 1081.30 2.706 546 1080.20 2.703 538 903.56 2.261 264 901.86 2.257 388 900.27 2.253 294 898.32 2.248 137 892.70 2.234 292 891.11 2.230 429 889.40 2.226 326 887.57 2.221 146 800.66 2.004 161 796.14 1.993 145 791.87 1.982 355 786.99 1.970 350 783.33 1.961 225 779.54 1.951 231 776.25 1.943 250 774.78 1.939 259 771.61 1.931 222 760.25 1.903 168 756.47 1.893 277 752.08 1.882 174 748.41 1.873 199 744.02 1.862 407 739.87 1.852 279 735.47 1.841 126 731.08 1.830 149 656.62 1.643 242 655.40 1.640 309 654.79 1.639 325 653.56 1.636 476 652.34 1.633 347 651.86 1.632 333 650.51 1.628 284 645.87 1.617 240 644.53 1.613 300 643.92 1.612 310 642.82 1.609 453 641.60 1.606 333 640.99 1.604 320 639.77 1.601 270 635.25 1.590 169 633.06 1.585 184 629.76 1.576 125 626.46 1.568 224 624.15 1.562 260 623.05 1.559 358 620.85 1.554 332 613.65 1.536 766 611.45 1.530 866 604.25 1.512 263 602.05 1.507 294 600.34 1.503 260 598.02 1.497 214 591.67 1.481 142 589.36 1.475 132
in CDCl3
liquid film
