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网站主页CAS数据库列表 30339-30-1更多图谱(S)-1-苯基-2-对甲苯基乙胺(30339-30-1)核磁图(1HNMR)

(S)-1-苯基-2-对甲苯基乙胺

产品名称 (S)-1-苯基-2-对甲苯基乙胺

CAS号30339-30-1

分子式C15H17N

分子量211.3

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  • Mass

    MS-IW-4061          
    (S)-1-phenyl-2-(p-tolyl)ethylamine
    C15H17N             (Mass of molecular ion:    211)
    

       Source Temperature: 230 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          28.0       6.2
          51.0       1.0
          77.0       7.4
          78.0       1.5
          79.0      18.0
          80.0       1.2
          91.0       2.4
         103.0       1.2
         104.0       3.1
         105.0       4.1
         106.0     100.0
         107.0       8.2
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C15 H17 N 0.05 ml : 0.5 ml CDCl3
    (S)-1-phenyl-2-(p-tolyl)ethylamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.34 B 7.32 C 7.231 D *1 7.08 E *1 7.05 F 4.146 G *2 2.962 J *2 2.773 K 2.301 L 1.9 J(G,F)=4.8HZ J(G,J)=-13.3HZ J(J,F)=8.9HZ

         Hz     ppm     Int.
    

       2939.45   7.356     89
       2937.62   7.351    119
       2935.42   7.345     63
       2934.45   7.343     55
       2931.03   7.334    417
       2928.83   7.329    440
       2928.22   7.327    392
       2925.90   7.322     70
       2922.00   7.312    259
       2921.26   7.310    332
       2919.43   7.305    118
       2915.16   7.295     83
       2913.45   7.291    121
       2911.87   7.287     36
       2897.83   7.251     88
       2896.12   7.247    136
       2894.04   7.242     72
       2891.85   7.236     74
       2889.89   7.232    102
       2889.16   7.230    134
       2886.60   7.223     60
       2885.25   7.220     31
       2884.16   7.217     53
       2882.45   7.213     72
       2880.62   7.208     51
       2834.59   7.093    111
       2833.98   7.092    124
       2825.93   7.072    446
       2820.56   7.058    508
       2818.36   7.053    104
       2814.21   7.042     68
       2812.26   7.037    134
       1663.09   4.162     34
       1662.72   4.161     34
       1661.99   4.159     33
       1658.45   4.150     41
       1658.08   4.149     41
       1657.84   4.149     41
       1657.47   4.148     41
       1656.98   4.147     40
       1655.52   4.143     41
       1655.15   4.142     41
       1650.88   4.131     34
       1650.63   4.131     34
       1193.85   2.988     52
       1189.09   2.976     52
       1180.54   2.954     73
       1175.66   2.942     69
       1118.41   2.799    100
       1109.50   2.777     98
       1104.98   2.765     75
       1096.07   2.743     71
        919.80   2.302   1000
    

(at 60.C)



liquid film