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哌啶基乙腈

产品名称 哌啶基乙腈

CAS号3010-03-5

分子式C7H12N2

分子量124.18

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  • Mass

    MS-IW-4780          
    piperidinoacetonitrile
    C7H12N2             (Mass of molecular ion:    124)
    

       Source Temperature: 210 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          15.0       2.1
          26.0       2.1
          27.0      11.1
          28.0       9.0
          29.0       5.8
          30.0       2.3
          39.0       7.7
          40.0       5.7
          41.0      23.6
          42.0      23.3
          43.0      19.0
          44.0       1.7
          51.0       1.3
          52.0       2.2
          53.0       2.7
          54.0       5.0
          55.0      14.2
          56.0       8.7
          57.0       6.4
          66.0       1.2
          67.0      10.8
          68.0      10.7
          69.0       9.0
          70.0       2.6
          79.0       2.1
          80.0       1.6
          81.0       1.8
          82.0      21.8
          83.0      27.6
          84.0      12.0
          85.0       1.2
          94.0       1.4
          95.0       7.0
          96.0      15.1
          97.0       5.9
          98.0       5.4
         109.0       3.0
         123.0     100.0
         124.0      38.6
         125.0       3.0
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C7 H12 N2 0.05 ml : 0.5 ml CDCl3
    piperidinoacetonitrile
    ChemicalStructure
        Assign.     Shift(ppm)
    A 3.502 B 2.520 C 1.626 D 1.454

         Hz     ppm     Int.
    

       1399.78   3.503   1000
       1396.97   3.496     65
       1396.00   3.494     40
       1012.57   2.534    301
       1007.20   2.521    364
       1001.59   2.507    274
        661.38   1.655    127
        655.64   1.641    235
        650.02   1.627    321
        644.29   1.613    257
        638.67   1.599    137
        591.80   1.481     62
        585.69   1.466    123
        580.08   1.452    145
        574.10   1.437     83
        568.48   1.423     34
    

in CDCl3



liquid film