400 MHz in DMSO-d6
-
1H NMR 399.65 MHz C18 H17 N6 Na O5 S2 0.038 g : 0.5 ml DMSO-d6 cefamandole sodium 
Assign. Shift(ppm)
A 8.62 B 7.444 C 7.317 D 7.262 E 6.32 F 5.549 G 5.12 J 4.943 K *1 4.417 L *1 4.236 M 3.915 N *2 3.571 P *2 3.395 J(A,F)=9.2 HZ J(F,J)=4.9 HZ J(K,L)=-12.5 HZ J(N,P)=-17.7 HZ ASSIGNED BY H-H COSY.
Hz ppm Int.3448.49 8.629 62 3439.33 8.606 66 2980.59 7.459 73 2978.88 7.454 105 2971.92 7.437 140 2933.35 7.340 43 2932.01 7.337 69 2924.93 7.319 157 2923.46 7.316 76 2918.82 7.304 48 2917.48 7.301 101 2908.94 7.279 38 2907.47 7.276 70 2906.13 7.272 40 2900.27 7.258 79 2224.85 5.567 45 2220.09 5.556 51 2215.82 5.545 47 2210.94 5.533 48 2046.02 5.120 60 1977.78 4.949 155 1972.90 4.937 138 1772.09 4.435 66 1759.77 4.404 80 1698.49 4.250 71 1686.04 4.219 55 1564.70 3.916 1000 1437.62 3.598 50 1419.92 3.553 70
in DMSO-d6
KBr disc
nujol mull
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