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网站主页CAS数据库列表 2987-53-3更多图谱2-氨基茴香硫醚(2987-53-3)Raman光谱

2-氨基茴香硫醚

产品名称 2-氨基茴香硫醚

CAS号2987-53-3

分子式C7H9NS

分子量139.22

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  • Mass

    MS-IW-7539          
    o-(methylthio)aniline
    C7H9NS              (Mass of molecular ion:    139)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          28.0       2.4
          38.0       1.5
          39.0       5.0
          41.0       1.0
          45.0       4.6
          50.0       1.0
          51.0       1.8
          52.0       3.0
          53.0       4.5
          54.0       1.1
          61.5       1.6
          62.0       1.4
          63.0       3.8
          64.0       2.3
          65.0       7.1
          66.0       2.5
          67.0       1.2
          69.0       2.8
          69.5       3.2
          70.0       1.8
          77.0       2.4
          78.0       1.5
          80.0      40.8
          81.0       2.6
          90.0       1.2
          91.0       2.8
          92.0       1.9
          93.0       4.4
          94.0       5.4
          95.0       1.4
          96.0       2.7
          97.0       8.8
         106.0       9.2
         108.0       1.6
         109.0       1.1
         122.0       1.0
         124.0      94.6
         125.0       7.5
         126.0       4.6
         135.0       2.6
         139.0     100.0
         140.0       9.3
         141.0       4.9
         149.0       1.7
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C7 H9 N S 0.05 ml : 0.5 ml CDCl3
    o-(methylthio)aniline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.318 B 7.046 C 6.68 D 6.64 E 4.15 F 2.297

         Hz     ppm     Int.
    

       2929.81   7.331     89
       2929.44   7.331     88
       2928.22   7.327     95
       2922.12   7.312     96
       2921.75   7.311     96
       2920.53   7.308    102
       2824.71   7.068     67
       2823.24   7.065     68
       2817.38   7.050     89
       2816.77   7.049     93
       2815.80   7.046     88
       2815.31   7.045     85
       2809.45   7.030     88
       2807.86   7.026     82
       2677.73   6.701     69
       2676.39   6.697     82
       2670.41   6.682     92
       2669.07   6.679    110
       2662.72   6.663     68
       2661.38   6.660    105
       2661.01   6.659    120
       2660.52   6.658    120
       2659.67   6.655    100
       2652.95   6.639    101
       2652.59   6.638    105
       2651.61   6.635     96
       2651.25   6.634     87
       1659.42   4.153     31
        918.21   2.298   1000
    

in CDCl3



liquid film