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网站主页CAS数据库列表 29815-94-9更多图谱双(4-氯苯氧基)乙酸(29815-94-9)核磁图(13CNMR)

双(4-氯苯氧基)乙酸

产品名称 双(4-氯苯氧基)乙酸

CAS号29815-94-9

分子式C14H10Cl2O4

分子量313.13


  • Mass

    MS-NW-8067          
    bis(p-chlorophenoxy)acetic acid
    C14H10Cl2O4         (Mass of molecular ion:    312)
    

       Source Temperature: 190 °C
       Sample Temperature: 140 °C
       Direct, 75 eV
    

          18.0       1.3
          28.0       1.5
          29.0       3.9
          36.0       1.1
          38.0       2.1
          39.0       4.3
          44.0       1.7
          45.0       1.2
          50.0       7.4
          51.0       5.6
          61.0       1.3
          62.0       1.7
          63.0       6.7
          64.0       3.9
          65.0      11.8
          66.0       1.3
          73.0       6.1
          74.0       3.1
          75.0      33.5
          76.0       7.1
          77.0       4.8
          85.0       2.9
          87.0       1.0
          93.0      16.0
          94.0       9.6
          99.0       8.8
         100.0       3.1
         101.0       3.5
         102.0       1.0
         111.0      56.5
         112.0       4.6
         113.0      19.1
         114.0       1.6
         127.0       4.7
         128.0     100.0
         129.0      32.0
         130.0      33.4
         131.0       9.9
         132.0       1.3
         139.0       4.6
         140.0       1.0
         141.0       4.5
         143.0       1.0
         150.0       1.5
         157.0       7.5
         159.0       2.5
         167.0      44.9
         168.0       5.5
         169.0      14.9
         170.0       1.5
         185.0      74.7
         186.0       7.4
         187.0      24.5
         188.0       2.4
         204.0       1.6
         267.0      10.0
         268.0       1.7
         269.0       6.4
         270.0       1.0
         271.0       1.1
         312.0      32.6
         313.0       5.1
         314.0      21.4
         315.0       3.3
         316.0       3.8
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C14 H10 Cl2 O4 0.034 g : 0.5 ml DMSO-d6
    bis(p-chlorophenoxy)acetic acid
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.382 B 7.099 C 6.481

         Hz     ppm     Int.
    

       2958.98   7.404     71
       2955.57   7.396    811
       2953.13   7.390    268
       2951.17   7.385     43
       2950.68   7.384     43
       2948.73   7.379    274
       2946.29   7.373   1000
       2942.87   7.364    107
       2844.97   7.119     87
       2841.55   7.111    981
       2839.36   7.105    262
       2834.72   7.094    251
       2832.52   7.088    812
       2828.86   7.079     80
       2590.33   6.482    569
    

in DMSO-d6



KBr disc



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