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MassMS-NW-6637 4-(1-butylpentyl)pyridine C14H23N (Mass of molecular ion: 205)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
18.0 1.9 27.0 10.7 29.0 15.1 39.0 8.5 40.0 1.0 41.0 18.6 42.0 1.4 43.0 10.8 50.0 1.3 51.0 5.7 52.0 4.0 53.0 2.9 54.0 1.7 55.0 4.7 56.0 1.3 57.0 7.1 63.0 1.7 65.0 10.1 66.0 1.3 67.0 1.1 69.0 1.2 77.0 6.6 78.0 6.0 79.0 4.4 80.0 3.3 81.0 1.1 91.0 4.5 92.0 30.3 93.0 30.6 94.0 3.9 95.0 1.2 104.0 4.1 105.0 12.2 106.0 91.5 107.0 12.9 108.0 1.4 117.0 5.2 118.0 11.2 119.0 8.8 120.0 11.0 121.0 6.8 122.0 2.1 130.0 1.6 132.0 4.1 133.0 5.6 134.0 4.8 135.0 1.0 146.0 1.6 147.0 2.9 148.0 100.0 149.0 90.8 150.0 10.7 162.0 15.1 163.0 5.7 176.0 2.4 190.0 1.5 204.0 1.8 205.0 40.9 206.0 7.1
90 MHz in CDCl3
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1H NMR 89.56 MHz C14 H23 N 0.05 ml : 0.5 ml CDCl3 4-(1-butylpentyl)pyridine 
Assign. Shift(ppm)
A 8.482 B 7.063 C 2.41 D 1.58 E 1.20 F 0.83
Hz ppm Int.763.06 8.521 361 761.44 8.503 236 758.63 8.471 248 757.00 8.453 392 635.56 7.097 388 634.00 7.080 252 631.06 7.047 238 629.50 7.029 354 221.81 2.477 74 143.69 1.605 245 138.63 1.548 247 138.06 1.542 249 107.06 1.196 479 104.19 1.164 429 100.38 1.121 414 80.00 0.894 494 73.94 0.826 1000 67.56 0.755 253
in CDCl3
liquid film
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