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MassMS-NW-9701 2-amino-2',5-dichlorobenzophenone C13H9Cl2NO (Mass of molecular ion: 265)
Source Temperature: 150 °C Sample Temperature: 80 °C Direct, 75 eV
39.0 1.0 50.0 1.2 51.0 1.3 52.0 1.4 62.0 1.3 63.0 4.8 64.0 1.5 65.0 1.1 73.0 1.7 74.0 1.4 75.0 7.2 76.0 1.3 82.5 1.4 83.5 1.0 90.0 6.4 91.0 2.8 99.0 7.4 100.0 1.1 100.5 1.9 101.0 2.8 111.0 14.6 112.0 1.2 113.0 5.2 115.0 5.5 115.5 1.0 116.0 1.8 125.0 1.6 126.0 14.0 127.0 1.7 128.0 4.6 138.0 1.1 139.0 22.2 140.0 3.4 141.0 6.6 153.0 2.4 154.0 28.9 155.0 3.1 156.0 9.6 164.0 1.6 165.0 1.1 166.0 6.2 167.0 8.9 168.0 1.5 194.0 1.8 195.0 24.9 196.0 3.8 200.0 1.7 201.0 5.2 202.0 2.5 203.0 1.9 229.0 12.1 230.0 100.0 231.0 18.2 232.0 32.7 233.0 4.7 236.0 4.1 238.0 2.6 248.0 3.7 250.0 2.4 264.0 18.6 265.0 56.4 266.0 19.9 267.0 36.6 268.0 7.0 269.0 6.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C13 H9 Cl2 N O 0.036 g : 0.5 ml CDCl3 2-amino-2',5-dichlorobenzophenone 
Assign. Shift(ppm)
A 7.459 B 7.414 C 7.341 D 7.300 E 7.225 F 7.114 G 6.669 J 6.42
Hz ppm Int.2987.43 7.476 274 2986.94 7.474 299 2985.84 7.472 372 2983.40 7.466 74 2979.61 7.456 619 2979.00 7.455 685 2978.03 7.452 748 2977.54 7.451 705 2971.31 7.435 401 2969.60 7.431 417 2964.11 7.417 617 2962.40 7.413 629 2958.74 7.404 81 2956.30 7.398 368 2954.35 7.393 381 2950.20 7.382 410 2948.61 7.378 397 2946.78 7.374 83 2942.75 7.364 663 2941.28 7.360 683 2937.87 7.352 76 2937.38 7.350 75 2935.55 7.346 374 2934.08 7.342 354 2930.42 7.333 39 2925.17 7.320 52 2921.14 7.310 601 2920.65 7.309 644 2919.31 7.305 584 2918.82 7.304 578 2913.33 7.290 425 2911.87 7.287 359 2897.46 7.250 38 2893.31 7.240 547 2890.87 7.234 609 2884.52 7.218 590 2881.96 7.212 656 2844.36 7.118 985 2841.92 7.112 911 2675.29 6.695 30 2669.68 6.681 1000 2666.99 6.674 84 2665.41 6.670 63 2663.70 6.666 74 2660.77 6.658 953 2586.55 6.473 311
in CDCl3
KBr disc
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