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MassMS-IW-1288 4'-bromo-4-biphenylol C12H9BrO (Mass of molecular ion: 248)
Source Temperature: 150 °C Sample Temperature: 110 °C Direct, 75 eV
18.0 2.5 39.0 1.5 50.0 1.0 51.0 1.2 55.0 1.2 62.0 1.1 63.0 2.2 69.0 1.0 69.5 1.5 70.0 1.7 70.5 1.0 75.0 1.4 84.0 5.4 84.5 2.3 89.0 1.4 113.0 1.3 114.0 1.7 115.0 7.6 124.0 3.1 125.0 3.1 139.0 9.8 140.0 4.7 141.0 18.3 142.0 2.5 151.0 2.4 152.0 1.9 168.0 7.1 169.0 4.7 219.0 1.6 221.0 1.5 247.0 1.1 248.0 100.0 249.0 14.3 250.0 99.0 251.0 12.9 252.0 1.0
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C12 H9 Br O 0.035 g : 0.5 ml DMSO-d6 4'-bromo-4-biphenylol 
Assign. Shift(ppm)
A 9.67 B 7.580 C 7.538 D 7.496 E 6.874
Hz ppm Int.3867.03 9.677 1000 3037.41 7.601 69 3035.28 7.595 408 3032.99 7.590 166 3028.72 7.579 233 3026.43 7.573 946 3024.29 7.568 202 3020.17 7.558 53 3017.58 7.551 193 3015.44 7.546 920 3013.15 7.540 243 3008.88 7.529 173 3006.59 7.524 408 3004.46 7.518 96 3003.54 7.516 103 3000.49 7.508 603 2998.35 7.503 214 2996.06 7.497 67 2993.93 7.492 208 2991.79 7.487 646 2988.74 7.479 89 2754.52 6.893 87 2751.62 6.886 704 2749.48 6.880 221 2744.90 6.869 207 2742.77 6.863 654 2739.87 6.856 83
in DMSO-d6
KBr disc
nujol mull
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