-
MassMS-NW-8773 2-biphenylmethanol C13H12O (Mass of molecular ion: 184)
Source Temperature: 280 °C Sample Temperature: 150 °C Reservoir, 75 eV
18.0 2.2 27.0 1.6 28.0 1.5 39.0 3.8 50.0 2.6 51.0 8.8 52.0 1.8 55.0 1.4 62.0 1.5 63.0 5.8 64.0 2.6 65.0 1.9 69.5 2.5 74.0 2.2 75.0 3.4 75.5 1.0 76.0 9.7 76.5 1.7 77.0 20.2 78.0 11.3 79.0 8.3 81.0 1.1 81.5 1.8 82.0 6.7 82.5 7.9 83.0 5.0 87.0 1.5 89.0 2.8 90.0 1.2 91.0 6.3 91.5 2.2 92.0 2.2 101.0 1.4 102.0 2.7 103.0 1.1 105.0 9.7 106.0 2.0 107.0 8.2 113.0 1.0 115.0 11.7 116.0 2.4 118.0 1.8 126.0 3.1 127.0 5.8 128.0 9.0 129.0 5.5 130.0 1.5 139.0 4.0 141.0 7.8 142.0 1.6 143.0 1.2 150.0 2.4 151.0 6.9 152.0 23.5 153.0 16.3 154.0 7.5 155.0 43.5 156.0 10.0 157.0 1.8 163.0 3.2 164.0 4.8 165.0 78.5 166.0 67.7 167.0 17.6 168.0 3.1 169.0 8.8 170.0 1.2 181.0 5.6 182.0 2.3 183.0 22.3 184.0 100.0 185.0 14.1 186.0 1.1
400 MHz in CDCl3
-
1H NMR 399.65 MHz C13 H12 O 0.036 g : 0.5 ml CDCl3 2-biphenylmethanol 
Assign. Shift(ppm)
A 7.52 B 7.40 C 7.35 D 7.34 E 7.33 F 7.268 G 4.576 J 1.80 ASSIGNED BY H-H AND C-H COSY. CONFIRMED BY LAOCN PROGRAM.
Hz ppm Int.3012.45 7.538 187 3011.96 7.537 197 3010.25 7.533 248 3006.23 7.523 93 3005.49 7.521 170 3004.64 7.519 198 3004.03 7.517 192 3003.42 7.516 256 3002.93 7.514 244 2971.44 7.436 35 2971.07 7.435 36 2970.09 7.432 41 2968.99 7.429 58 2967.77 7.426 149 2966.19 7.422 208 2964.97 7.419 127 2964.48 7.418 138 2961.79 7.411 168 2960.57 7.408 303 2958.74 7.404 341 2958.25 7.403 310 2957.40 7.400 367 2956.18 7.397 161 2955.08 7.395 207 2952.15 7.387 685 2951.42 7.386 732 2950.07 7.382 232 2946.17 7.372 418 2944.21 7.367 546 2942.87 7.364 490 2939.94 7.357 563 2939.21 7.355 976 2938.48 7.353 1000 2937.74 7.351 758 2937.13 7.350 810 2936.16 7.347 552 2932.74 7.339 559 2931.15 7.335 654 2929.57 7.331 420 2928.22 7.327 138 2927.37 7.325 96 2925.29 7.320 178 2923.58 7.316 142 2920.90 7.309 33 2919.92 7.307 39 2918.09 7.302 34 2915.04 7.294 33 2914.43 7.293 31 2912.35 7.288 34 2908.81 7.279 321 2907.35 7.275 250 2906.37 7.273 211 2901.73 7.261 293 2899.66 7.256 185 1828.86 4.577 798 718.75 1.799 220
in CDCl3
KBr disc
nujol mull
4880 A,200 M,powder
更多供应商
