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MassMS-NW-6879 m-fluorophenylhydrazine hydrochloride C6H7FN2 HCl (Mass of molecular ion: 126)
Source Temperature: 180 °C Sample Temperature: 120 °C Direct, 75 eV
17.0 1.1 18.0 4.2 27.0 1.2 28.0 2.3 29.0 8.1 30.0 2.4 31.0 5.4 35.0 5.9 36.0 26.4 37.0 2.8 38.0 8.7 39.0 4.8 49.0 1.1 50.0 6.9 51.0 6.6 52.0 3.2 56.0 1.9 57.0 11.8 61.0 2.5 62.0 4.0 63.0 8.2 64.0 2.5 65.0 1.2 68.0 2.4 69.0 3.9 70.0 5.4 71.0 1.6 74.0 3.5 75.0 12.2 76.0 1.9 77.0 9.1 78.0 1.8 79.0 1.0 81.0 4.2 82.0 8.4 83.0 41.8 84.0 4.7 89.0 3.2 90.0 2.2 94.0 1.5 95.0 14.3 96.0 18.9 97.0 9.1 98.0 4.4 99.0 1.9 108.0 1.8 109.0 18.5 110.0 28.0 111.0 10.4 124.0 1.2 125.0 5.6 126.0 100.0 127.0 7.3
400 MHz in DMSO-d6
90 MHz in DMSO-d6
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1H NMR 399.65 MHz C6 H7 F N2 0.021 g : 0.5 ml DMSO-d6 m-fluorophenylhydrazine hydrochloride 
Assign. Shift(ppm)
A 10.50 B 8.7 C 7.297 D 6.874 E 6.831 G 6.730
Hz ppm Int.4197.26 10.503 1000 2933.41 7.340 33 2933.05 7.340 40 2932.50 7.338 34 2931.95 7.337 32 2931.58 7.336 34 2931.03 7.334 38 2930.48 7.333 44 2930.11 7.332 50 2928.10 7.327 311 2924.80 7.319 83 2924.25 7.318 78 2921.14 7.310 388 2920.04 7.307 715 2913.26 7.290 657 2911.80 7.286 546 2907.77 7.276 75 2907.40 7.275 72 2905.02 7.269 342 2902.27 7.263 50 2764.17 6.917 30 2761.42 6.910 33 2761.05 6.909 33 2760.69 6.908 37 2760.32 6.907 37 2759.95 6.906 38 2759.40 6.905 47 2759.04 6.904 49 2758.67 6.903 56 2755.92 6.896 345 2753.73 6.891 665 2751.53 6.885 480 2747.50 6.875 104 2744.57 6.868 347 2743.83 6.866 306 2742.37 6.862 670 2740.17 6.857 521 2737.24 6.850 161 2734.86 6.844 752 2733.39 6.840 615 2732.66 6.838 612 2726.62 6.823 643 2725.33 6.820 581 2724.60 6.818 577 2719.11 6.804 33 2705.37 6.770 30 2705.00 6.769 30 2703.90 6.766 40 2703.35 6.765 44 2699.32 6.755 334 2696.94 6.749 329 2694.75 6.743 123 2693.83 6.741 107 2690.53 6.733 566 2688.70 6.728 579 2685.22 6.719 104 2682.29 6.712 322 2680.46 6.708 290 2679.73 6.706 293 2677.34 6.700 56
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1H NMR 89.56 MHz C6 H7 F N2 0.034 g : 0.5 ml DMSO-d6 m-fluorophenylhydrazine hydrochloride Assign. Shift(ppm)
A 10.5 B 7.283 C 6.98 to 6.78 D 6.72
Hz ppm Int.942.19 10.521 451 665.58 7.432 185 658.83 7.357 253 657.36 7.340 453 650.32 7.262 444 649.74 7.255 417 642.26 7.172 311 625.24 6.982 251 623.19 6.959 480 620.99 6.934 439 617.18 6.892 604 616.30 6.882 606 614.10 6.857 482 611.75 6.831 864 609.70 6.808 1000 605.59 6.762 219 603.24 6.736 501 601.04 6.712 390 595.03 6.644 230 593.42 6.626 200 592.98 6.622 201
KBr disc
nujol mull
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