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网站主页CAS数据库列表 2922-28-3更多图谱腺嘌呤盐酸盐(2922-28-3)核磁图(13CNMR)

腺嘌呤盐酸盐

产品名称 腺嘌呤盐酸盐

CAS号2922-28-3

分子式C5H6ClN5

分子量171.59

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  • Mass

    MS-NW-0241          
    adenine hydrochloride
    C5H5N5 HCl          (Mass of molecular ion:    135)
    

       Source Temperature: 200 °C
       Sample Temperature:   0 °C
       Direct, 75 eV
    

          17.0       3.9
          18.0      15.8
          27.0       3.0
          28.0      29.3
          29.0       6.0
          35.0      11.2
          36.0      62.5
          37.0       4.0
          38.0      22.0
          39.0       3.9
          40.0       2.8
          43.0       5.4
          53.0      12.3
          54.0      14.1
          55.0       3.0
          56.0       1.4
          64.0       1.6
          65.0       2.5
          66.0       8.2
          67.0       2.5
          68.0       3.0
          70.0       3.4
          80.0       3.7
          81.0      11.0
          92.0       1.9
          93.0       1.1
         107.0       2.1
         108.0      29.6
         109.0       2.2
         118.0       1.0
         119.0       1.1
         134.0       3.6
         135.0     100.0
         136.0       7.1
    

400 MHz DMSO-d6

90 MHz in D2O


  • 1H NMR 399.65 MHz
    C5 H5 N5 0.039 g : 0.5 ml DMSO-d6
    adenine hydrochloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 9.5 B *1 9.1 C 8.632 D 8.610

         Hz     ppm     Int.
    

       3801.27   9.512     36
       3648.99   9.131     35
       3449.86   8.633    911
       3441.31   8.611   1000
    


  • 1H NMR 89.56 MHz
    C5 H5 N5 saturated in D2O
    adenine hydrochloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.480 B 8.420 SOLVENT PEAK REMOVED

         Hz     ppm     Int.
    

        764.13   8.533     39
        763.50   8.526     43
        763.19   8.522     51
        759.56   8.482   1000
        757.00   8.453    107
        754.19   8.422    970
        751.75   8.394     72
        751.44   8.391     68
        750.31   8.378     55
        749.56   8.370     54
        748.44   8.357     45
        747.88   8.351     39
    

in D2O



KBr disc



nujol mull