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MassMS-IW-1290 (trimethylsilyl)methyl acetate C6H14O2Si (Mass of molecular ion: 146)
Source Temperature: 240 °C Sample Temperature: 160 °C Reservoir, 75 eV
15.0 1.5 28.0 1.0 29.0 2.4 31.0 1.6 42.0 1.5 43.0 27.5 44.0 3.6 45.0 13.1 47.0 2.1 55.0 1.1 57.0 1.1 58.0 2.8 59.0 5.9 60.0 1.3 61.0 51.0 62.0 3.2 63.0 1.8 72.0 4.9 73.0 100.0 74.0 9.8 75.0 7.9 89.0 24.7 90.0 2.1 91.0 1.2 101.0 9.1 103.0 13.6 104.0 9.6 105.0 1.9 116.0 9.7 117.0 1.1 131.0 31.0 132.0 3.3 133.0 1.4
400 MHz in CDCl3
in CDCl3
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1H NMR 399.65 MHz C6 H14 O2 Si 0.05 ml : 0.5 ml CDCl3 (trimethylsilyl)methyl acetate 
Assign. Shift(ppm)
A 3.761 B 2.041 C 0.078
Hz ppm Int.1503.30 3.762 481 815.67 2.041 661 35.03 0.088 205 31.62 0.080 962 31.13 0.078 1000 28.20 0.071 300
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in CDCl3
liquid film
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