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MS-NW-7561 p-tert-butyl-N,N-dimethylaniline C12H19N (Mass of molecular ion: 177)
Source Temperature: 260 °C Sample Temperature: 170 °C Reservoir, 75 eV
39.0 1.7 41.0 2.0 42.0 1.7 51.0 1.4 63.0 1.0 65.0 1.2 66.5 3.9 67.0 1.0 72.5 1.8 77.0 3.1 78.0 1.0 79.0 1.0 81.0 1.9 91.0 3.1 103.0 1.5 104.0 1.0 105.0 1.1 106.0 1.0 107.0 1.0 115.0 1.7 116.0 1.0 117.0 1.9 118.0 2.7 120.0 3.2 121.0 3.3 122.0 2.4 130.0 1.6 131.0 1.1 132.0 1.4 134.0 4.2 144.0 1.1 145.0 1.3 146.0 7.4 147.0 12.4 148.0 2.5 160.0 4.2 161.0 3.3 162.0 100.0 163.0 12.7 176.0 1.9 177.0 27.7 178.0 3.9
90 MHz in CDCl3
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1H NMR 89.56 MHz C12 H19 N 0.05 ml : 0.5 ml CDCl3 p-tert-butyl-N,N-dimethylaniline Assign. Shift(ppm)
A 7.254 B 6.703 C 2.880 D 1.286
Hz ppm Int.
654.94 7.313 65 652.63 7.288 24 648.25 7.239 29 645.94 7.213 91 603.88 6.743 83 601.56 6.717 25 597.13 6.668 22 594.88 6.643 57 258.00 2.881 685 115.25 1.287 1000
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