-
MassMS-NW-6374 N,N'-diallyltartardiamide C10H16N2O4 (Mass of molecular ion: 228)
Source Temperature: 140 °C Sample Temperature: 110 °C Direct, 75 eV
15.0 1.8 18.0 5.2 27.0 2.8 28.0 11.1 29.0 3.5 30.0 9.0 31.0 4.8 39.0 14.1 40.0 1.5 41.0 63.7 42.0 4.8 43.0 3.8 44.0 3.3 54.0 2.0 55.0 3.2 56.0 16.8 57.0 31.3 58.0 15.7 59.0 1.3 60.0 5.7 61.0 5.4 68.0 2.1 69.0 2.9 70.0 1.0 71.0 6.6 74.0 5.5 84.0 47.1 85.0 3.7 86.0 1.7 97.0 1.1 98.0 3.2 99.0 1.7 112.0 2.8 114.0 1.5 115.0 16.5 116.0 1.2 127.0 4.0 128.0 5.8 144.0 100.0 145.0 9.6 146.0 1.3 172.0 1.0 228.0 1.3
400 MHz in DMSO-d6
-
1H NMR 399.65 MHz C10 H16 N2 O4 0.039 g : 0.5 ml DMSO-d6 N,N'-diallyltartardiamide 
Assign. Shift(ppm)
A 7.81 B 5.804 C 5.62 D 5.159 E 5.034 F 4.27 G 3.75
Hz ppm Int.3127.56 7.826 387 3121.70 7.812 771 3115.60 7.796 393 2339.23 5.854 224 2334.23 5.841 539 2332.03 5.836 60 2329.10 5.828 423 2323.85 5.815 619 2322.02 5.811 307 2318.97 5.803 297 2317.02 5.798 659 2311.89 5.785 474 2306.64 5.772 641 2301.64 5.760 271 2249.63 5.630 504 2242.92 5.613 461 2076.78 5.197 35 2076.29 5.196 33 2072.51 5.186 341 2070.80 5.182 964 2068.97 5.177 1000 2067.14 5.173 347 2063.60 5.164 31 2061.40 5.159 36 2059.57 5.154 38 2055.30 5.143 300 2053.47 5.139 854 2051.76 5.134 868 2049.93 5.130 302 2019.53 5.054 356 2017.94 5.050 984 2016.24 5.046 923 2014.53 5.041 328 2011.60 5.034 80 2009.28 5.028 350 2007.57 5.024 905 2005.86 5.020 901 2004.27 5.016 313 2001.22 5.008 43 1999.51 5.004 34 1708.74 4.276 666 1702.76 4.261 657 1509.64 3.778 84 1506.47 3.770 278 1504.76 3.766 509 1501.83 3.758 698 1499.88 3.753 862 1498.66 3.750 903 1496.95 3.746 898 1495.97 3.744 873 1494.02 3.739 692 1490.97 3.731 499 1489.26 3.727 279 1486.08 3.719 95 1480.83 3.706 83 1480.10 3.704 80
in DMSO-d6
KBr disc
nujol mull
