3-甲基-5,6,7,8-四氢喹啉

产品名称 3-甲基-5,6,7,8-四氢喹啉

CAS号28712-62-1

分子式C10H13N

分子量147.22

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¹HNMR

¹³CNMR

IR1

Mass

MS-IW-1361          
3-methyl-5,6,7,8-tetrahydroquinoline
C10H13N             (Mass of molecular ion:    147)

   Source Temperature: 230 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      27.0       1.4
      39.0       4.8
      41.0       1.7
      50.0       1.5
      51.0       4.3
      52.0       2.3
      53.0       2.4
      63.0       2.6
      65.0       4.9
      65.5       1.3
      66.0       1.8
      71.5       1.3
      72.5       1.1
      77.0       8.1
      78.0       3.4
      79.0       3.3
      89.0       1.6
      90.0       1.0
      91.0       7.4
      92.0       2.4
      93.0       4.5
     103.0       2.2
     104.0       7.4
     105.0       2.1
     106.0       4.5
     107.0       1.5
     115.0       3.2
     116.0       1.5
     117.0       8.0
     118.0      10.2
     119.0      31.7
     120.0       4.6
     121.0       1.1
     128.0       1.2
     129.0       1.4
     130.0       7.8
     131.0      16.0
     132.0      34.2
     133.0       3.8
     143.0       2.3
     144.0      10.4
     145.0       3.4
     146.0     100.0
     147.0      96.6
     148.0      11.5

400 MHz in CDCl3

90 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₀ H₁₃ N	20.8 mg : 0.5 ml CDCl₃
3-methyl-5,6,7,8-tetrahydroquinoline

    Assign.     Shift(ppm)

      A             8.176
      B             7.157
      C             2.875
      D             2.721
      E             2.252
      F             1.873
      G             1.787

     Hz     ppm     Int.

   3268.07   8.178    166
   3267.33   8.176    163
   3266.72   8.174    168
   2860.96   7.159    173
   2860.47   7.158    171
   2859.99   7.157    172
   2859.50   7.156    171
   1155.27   2.891    116
   1149.05   2.876    240
   1142.58   2.859    139
   1093.75   2.737    129
   1087.65   2.722    234
   1081.18   2.706    125
    900.15   2.253   1000
    761.84   1.907     47
    758.54   1.899     45
    755.74   1.892    102
    752.69   1.884     91
    752.20   1.883    100
    750.49   1.878    151
    748.41   1.873     68
    746.70   1.869    107
    746.09   1.867     98
    744.38   1.863    177
    740.23   1.853     56
    737.92   1.847     75
    735.72   1.841     36
    726.93   1.819     35
    724.49   1.813     79
    722.53   1.808     64
    718.26   1.798    183
    716.43   1.793    110
    712.16   1.782    161
    711.18   1.780     92
    709.96   1.777     99
    707.28   1.770    110
    703.98   1.762     47
    701.17   1.755     42
    700.44   1.753     35

¹H NMR	89.56 MHz
C₁₀ H₁₃ N	0.04 ml : 0.5 ml CDCl₃
3-methyl-5,6,7,8-tetrahydroquinoline

    Assign.     Shift(ppm)

      A             8.170
      B             7.142
      C             2.87
      D             2.71
      E             2.244
      F          1.90 to 1.74
     
     400MHZ : HSP-40-251

     Hz     ppm     Int.

    732.50   8.179    169
    731.69   8.170    167
    730.88   8.161    171
    640.19   7.149    176
    639.63   7.142    174
    639.06   7.136    171
    262.69   2.934     86
    262.31   2.929     86
    262.00   2.926     85
    261.19   2.917     81
    257.13   2.872    190
    253.88   2.835     88
    253.50   2.831     87
    250.38   2.796    167
    246.63   2.754     83
    243.06   2.714    197
    238.13   2.659    127
    201.00   2.245   1000
    173.50   1.938     52
    173.13   1.934     50
    170.44   1.904    118
    168.75   1.885    126
    166.56   1.860    353
    163.81   1.830    286
    162.75   1.818    295
    159.88   1.786    341
    157.38   1.758    144
    155.63   1.738    114
    153.56   1.715     56
    153.19   1.711     55

in CDCl3

liquid film

更多供应商

3-甲基-5,6,7,8-四氢喹啉(28712-62-1)红外图谱(IR1) 相关产品图谱

伊匹达克林(62732-44-9)核磁图(¹HNMR) 1,2,3,4,5,6,7,8-八氢吖啶(1658-08-8)质谱(MS) 1,2,3,4,5,6,7,8-八氢吖啶(1658-08-8)核磁图(¹³CNMR) 1,2,3,4,5,6,7,8-八氢吖啶(1658-08-8)核磁图(¹HNMR) 1,2,3,4,5,6,7,8-八氢吖啶(1658-08-8)红外图谱(IR2)

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