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网站主页CAS数据库列表 287-08-1更多图谱环十五(碳)烯氧化物(287-08-1)核磁图(13CNMR)

环十五(碳)烯氧化物

产品名称 环十五(碳)烯氧化物

CAS号287-08-1

分子式C15H28O

分子量224.38

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  • Mass

    MS-KW-0170          
    16-oxabicyclo(13.1.0)hexadecane
    C15H28O             (Mass of molecular ion:    224)
    

       Source Temperature: 150 °C
       Sample Temperature: 110 °C
       Direct, 75 eV
    

          27.0      13.7
          28.0       3.7
          29.0      27.6
          31.0       2.0
          39.0      13.8
          40.0       2.7
          41.0      73.7
          42.0      13.4
          43.0      34.2
          44.0       6.1
          45.0       3.1
          53.0       7.8
          54.0      20.7
          55.0      93.8
          56.0      18.6
          57.0      38.9
          58.0       7.7
          59.0       3.1
          65.0       2.1
          66.0       8.5
          67.0      60.8
          68.0      46.8
          69.0      54.6
          70.0      19.6
          71.0      19.7
          72.0       3.4
          77.0       2.7
          78.0       1.8
          79.0      14.1
          80.0      35.3
          81.0      54.2
          82.0     100.0
          83.0      55.3
          84.0      14.2
          85.0       8.5
          86.0       1.4
          91.0       1.7
          93.0      13.8
          94.0      19.1
          95.0      41.7
          96.0      55.2
          97.0      36.7
          98.0      16.0
          99.0       3.2
         107.0       7.8
         108.0       8.2
         109.0      18.8
         110.0      16.2
         111.0      16.4
         112.0       5.1
         113.0       1.2
         121.0      14.9
         122.0       7.5
         123.0      10.5
         124.0      11.7
         125.0       6.8
         126.0       1.5
         135.0      11.6
         136.0       5.6
         137.0       6.8
         138.0       5.1
         139.0       2.1
         149.0       7.1
         150.0       3.0
         151.0       1.9
         152.0       1.7
         163.0       2.6
         164.0       1.5
         165.0       1.0
         166.0       1.3
         167.0       1.2
         177.0       1.3
         178.0       1.3
         180.0       1.4
         181.0       1.2
         196.0       1.3
         206.0       8.4
         207.0       2.2
         208.0       1.0
         224.0       6.8
         225.0       3.3
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C15 H28 O 0.036 g : 0.5 ml CDCl3
    16-oxabicyclo(13.1.0)hexadecane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.674 B 2.019 C 1.46 D 1.36 E 1.32 F 1.134

         Hz     ppm     Int.
    

       1076.42   2.694    144
       1074.46   2.689    361
       1071.78   2.682    295
       1070.80   2.680    211
       1066.89   2.670    213
       1065.92   2.668    301
       1063.23   2.661    374
       1061.28   2.656    136
        822.14   2.058     70
        819.09   2.050     88
        816.16   2.043    157
        813.11   2.035    156
        809.57   2.026    134
        806.64   2.019    137
        802.49   2.008    186
        799.56   2.001    171
        796.26   1.993    108
        793.21   1.985     93
        578.61   1.448    479
        526.86   1.319   1000
        470.70   1.178     85
        464.36   1.162    152
        462.16   1.157    105
        457.15   1.144    173
        455.81   1.141    172
        450.81   1.129    161
        449.10   1.124    159
        444.09   1.112    108
        442.14   1.107    136
        435.42   1.090     78
    

in CDCl3



KBr disk



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