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网站主页CAS数据库列表 2856-63-5更多图谱邻氯苯乙腈(2856-63-5)核磁图(1HNMR)

邻氯苯乙腈

产品名称 邻氯苯乙腈

CAS号2856-63-5

分子式C8H6ClN

分子量151.59

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  • Mass

    MS-NW-9213          
    (o-chlorophenyl)acetonitrile
    C8H6ClN             (Mass of molecular ion:    151)
    

       Source Temperature: 270 °C
       Sample Temperature: 160 °C
       Reservoir, 75 eV
    

          28.0       1.5
          37.0       1.8
          38.0       2.7
          39.0       5.9
          43.0       1.1
          49.0       1.2
          50.0       5.6
          51.0       3.8
          57.5       3.5
          61.0       2.7
          62.0       5.4
          63.0       8.8
          64.0       2.6
          65.0       1.6
          73.0       2.6
          74.0       2.9
          75.0       5.2
          75.5       1.0
          76.0       1.8
          85.0       1.3
          86.0       1.4
          87.0       2.8
          88.0       6.1
          89.0      19.3
          90.0       3.1
          99.0       1.3
         114.0       5.7
         115.0      15.2
         116.0     100.0
         117.0       9.1
         123.0       2.6
         124.0       1.7
         125.0       2.3
         150.0       2.7
         151.0      32.5
         152.0       3.9
         153.0      10.6
         154.0       1.0
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C8 H6 Cl N 0.05 ml : 0.5 ml CDCl3
    (o-chlorophenyl)acetonitrile
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.483 B 7.392 C 7.30 D 7.28 E 3.803

         Hz     ppm     Int.
    

       2995.85   7.497    142
       2992.80   7.489    114
       2991.46   7.486    159
       2990.11   7.482     83
       2988.77   7.479     94
       2986.57   7.473    172
       2959.59   7.406    173
       2957.15   7.400     96
       2954.59   7.393    181
       2953.13   7.390    146
       2950.32   7.383    250
       2946.53   7.373     40
       2922.36   7.313     74
       2920.17   7.307     44
       2917.36   7.300    387
       2914.79   7.294    224
       2912.60   7.288    345
       2909.91   7.282    177
       2907.96   7.277    296
       2904.54   7.268     31
       2901.86   7.262    122
       1520.14   3.804   1000
    

in CDCl3



liquid film