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MS-NW-8837 2-(cyclohexylamino)ethanol C8H17NO (Mass of molecular ion: 143)
Source Temperature: 270 °C Sample Temperature: 150 °C Reservoir, 75 eV
18.0 1.8 27.0 4.5 28.0 7.9 29.0 4.9 30.0 93.1 31.0 2.1 39.0 4.6 41.0 18.6 42.0 10.8 43.0 5.8 44.0 11.3 45.0 3.7 53.0 3.0 54.0 3.5 55.0 30.8 56.0 26.5 57.0 1.8 60.0 3.0 62.0 1.2 67.0 3.0 68.0 3.4 69.0 1.7 70.0 5.9 72.0 2.9 74.0 1.0 79.0 1.8 80.0 1.5 81.0 3.1 82.0 8.3 83.0 12.9 84.0 1.6 87.0 1.9 96.0 1.5 98.0 1.7 100.0 53.4 101.0 3.3 110.0 1.0 112.0 100.0 113.0 8.3 114.0 1.5 142.0 1.7 143.0 4.8 144.0 2.8
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H17 N O 0.025 g : 0.5 ml CDCl3 2-(cyclohexylamino)ethanol Assign. Shift(ppm)
A 3.646 B 2.86 C 2.781 D 2.431 E 1.902 F 1.734 G 1.619 J 1.25 K 1.20 L 1.08
Hz ppm Int.
1462.52 3.660 915 1459.47 3.652 263 1457.40 3.647 995 1455.20 3.642 293 1452.15 3.634 1000 1144.29 2.864 245 1121.95 2.808 41 1121.46 2.807 41 1116.70 2.795 964 1113.77 2.787 280 1111.45 2.782 990 1109.50 2.777 313 1106.32 2.769 925 986.21 2.468 84 982.42 2.459 173 978.64 2.449 110 975.71 2.442 186 971.92 2.432 360 968.14 2.423 207 965.09 2.415 118 961.30 2.406 195 957.64 2.397 104 768.55 1.924 268 765.99 1.917 285 762.21 1.908 181 760.99 1.905 181 755.98 1.892 291 753.17 1.885 300 706.54 1.768 72 703.25 1.760 209 699.58 1.751 300 695.92 1.742 236 689.94 1.727 264 686.40 1.718 351 684.20 1.712 247 657.23 1.645 122 655.40 1.640 147 654.17 1.637 183 652.59 1.633 133 650.76 1.629 134 649.41 1.625 117 645.26 1.615 143 642.58 1.608 183 641.72 1.606 188 640.26 1.603 126 638.31 1.598 140 634.77 1.589 57 525.02 1.314 66 521.73 1.306 95 518.43 1.298 47 512.94 1.284 179 509.64 1.276 292 506.71 1.268 160 499.88 1.251 235 497.07 1.244 398 494.26 1.237 235 489.87 1.226 59 487.43 1.220 163 484.25 1.212 257 482.42 1.208 211 480.83 1.204 218 477.54 1.195 140 471.56 1.180 132 468.63 1.173 265 465.33 1.165 152 462.40 1.158 44 459.96 1.151 82 456.54 1.143 185 453.25 1.135 100 448.36 1.122 166 444.70 1.113 173 440.67 1.103 79 435.91 1.091 307 433.84 1.086 303 425.42 1.065 251 422.97 1.059 274 413.70 1.036 89 410.28 1.027 101
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