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2,6-二氟苯酚

产品名称 2,6-二氟苯酚

CAS号28177-48-2

分子式C6H4F2O

分子量130.09

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  • Mass

    MS-IW-1278          
    2,6-difluorophenol
    C6H4F2O             (Mass of molecular ion:    130)
    

       Source Temperature: 250 °C
       Sample Temperature: 160 °C
       Reservoir, 75 eV
    

          31.0       3.7
          37.0       1.2
          38.0       1.1
          41.0       1.6
          50.0       2.0
          51.0       3.9
          53.0       1.5
          55.0       2.7
          56.0       3.5
          57.0       5.0
          61.0       1.7
          62.0       1.6
          63.0      13.4
          64.0       1.0
          65.0       4.1
          68.0       1.0
          75.0       4.4
          80.0       1.1
          81.0      15.8
          82.0      61.7
          83.0       4.4
          99.0       1.2
         101.0       8.1
         110.0      29.5
         111.0       2.0
         129.0       2.6
         130.0     100.0
         131.0       6.6
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C6 H4 F2 O 0.031 g : 0.5 ml CDCl3
    2,6-difluorophenol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.888 B 6.793 C 5.66

         Hz     ppm     Int.
    

       2772.22   6.937     60
       2770.26   6.932     68
       2764.40   6.918    105
       2763.06   6.914    365
       2761.72   6.911    647
       2760.38   6.907    317
       2756.35   6.897    331
       2754.27   6.892    810
       2753.78   6.891   1000
       2752.69   6.888    821
       2747.31   6.875    808
       2746.09   6.872    682
       2745.61   6.871    619
       2742.31   6.862     41
       2740.60   6.858     33
       2738.53   6.853    129
       2735.35   6.845     80
       2727.78   6.826    313
       2721.80   6.811    616
       2720.34   6.807    245
       2718.38   6.802    187
       2715.82   6.796    321
       2713.99   6.791    432
       2712.89   6.789    380
       2710.94   6.784    154
       2708.37   6.777    226
       2706.67   6.773    197
       2704.96   6.769    273
       2699.10   6.754    140
    

in CDCl3



KBr disc



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