3,5-二硝基-2-甲基苯甲酸

Mass

MS-NW-8263          
3,5-dinitro-o-toluic acid
C8H6N2O6            (Mass of molecular ion:    226)

   Source Temperature: 210 °C
   Sample Temperature: 140 °C
   Direct, 75 eV

      17.0       1.2
      18.0       5.0
      27.0       4.5
      28.0       6.6
      29.0       3.1
      30.0      27.2
      31.0       1.1
      37.0       2.4
      38.0       5.6
      39.0      29.4
      40.0       3.8
      41.0       1.7
      42.0       1.0
      43.0      14.7
      44.0       7.0
      45.0       7.2
      46.0       2.0
      49.0       1.2
      50.0      13.9
      51.0      35.3
      52.0      18.8
      53.0      13.8
      54.0       1.9
      55.0       6.5
      58.0       1.8
      61.0       5.8
      62.0      24.3
      63.0      55.5
      64.0      13.3
      65.0      12.2
      66.0      12.7
      67.0       7.5
      68.0       3.5
      69.0       4.5
      73.0       1.8
      74.0       8.7
      75.0      10.8
      76.0      11.2
      77.0      23.5
      78.0      26.4
      79.0      11.9
      80.0       6.8
      81.0       2.3
      82.0       1.9
      85.0       2.9
      86.0       8.3
      87.0      11.2
      88.0      11.9
      89.0      37.1
      90.0      21.4
      91.0       8.2
      92.0       7.7
      93.0       4.3
      94.0       6.3
      95.0       2.5
      96.0       1.3
     103.0       3.3
     104.0       4.6
     105.0      30.6
     106.0      28.6
     107.0      16.2
     108.0       5.3
     116.0      11.7
     117.0       5.6
     118.0     100.0
     119.0      22.0
     120.0       5.5
     121.0       8.2
     122.0       4.7
     123.0       1.4
     131.0       2.5
     132.0       3.3
     133.0      29.8
     134.0      25.5
     135.0      13.8
     136.0      27.6
     137.0       3.4
     145.0       5.2
     146.0       1.0
     148.0       5.1
     149.0       2.1
     150.0       5.0
     151.0       3.2
     152.0       2.8
     162.0       9.2
     163.0      15.4
     164.0       4.4
     165.0       6.4
     166.0       1.6
     167.0       2.4
     177.0       1.1
     179.0       9.9
     180.0       3.1
     181.0       1.8
     191.0      14.2
     192.0       3.7
     193.0       2.0
     196.0       1.0
     207.0       1.4
     208.0       1.0
     209.0      90.8
     210.0       9.7
     211.0       1.4
     226.0      31.0
     227.0       3.3

Assign. Shift(ppm) A 8.819 B 8.681 C 2.626

     Hz     ppm     Int.

    791.56   8.839    151
    791.13   8.834    158
    789.06   8.811    217
    788.63   8.806    219
    780.56   8.716     23
    778.75   8.696    227
    778.31   8.691    232
    776.25   8.668    158
    775.81   8.663    158
    235.25   2.627   1000