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网站主页CAS数据库列表 28034-99-3更多图谱4-氯联苯基-4-醇(28034-99-3)质谱(MS)

4-氯联苯基-4-醇

产品名称 4-氯联苯基-4-醇

CAS号28034-99-3

分子式C12H9ClO

分子量204.65

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  • Mass

    MS-IW-2677          
    4'-chloro-4-biphenylol
    C12H9ClO            (Mass of molecular ion:    204)
    

       Source Temperature: 110 °C
       Sample Temperature: 100 °C
       Direct, 75 eV
    

          18.0       1.1
          28.0       1.3
          39.0       1.8
          50.0       1.1
          51.0       1.5
          55.0       2.3
          62.0       1.3
          63.0       3.0
          69.0       1.8
          69.5       2.5
          70.0       3.1
          74.0       1.4
          75.0       2.4
          84.0       4.9
          84.5       1.1
          86.0       1.0
          87.0       1.2
          89.0       1.8
         102.0       6.2
         103.0       2.0
         113.0       1.7
         114.0       1.7
         115.0       6.3
         139.0       9.0
         140.0       3.3
         141.0      13.2
         142.0       1.8
         149.0       3.3
         151.0       2.2
         152.0       1.4
         168.0       5.3
         169.0       2.9
         175.0       3.1
         203.0       2.1
         204.0     100.0
         205.0      14.0
         206.0      33.0
         207.0       4.2
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C12 H9 Cl O saturated in CDCl3
    4'-chloro-4-biphenylol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.442 B 7.425 C 7.366 D 6.898 E 5.15

         Hz     ppm     Int.
    

       2982.18   7.462     67
       2979.74   7.456    485
       2977.66   7.451    200
       2974.98   7.444    103
       2973.14   7.440    296
       2972.05   7.437    752
       2970.95   7.434   1000
       2969.97   7.432    355
       2968.63   7.429    174
       2965.45   7.421    232
       2963.26   7.415    744
       2960.33   7.408     85
       2949.46   7.381    139
       2947.14   7.375    819
       2944.95   7.369    247
       2940.43   7.358    191
       2938.35   7.353    531
       2935.91   7.347     61
       2764.28   6.917     86
       2761.35   6.910    721
       2759.16   6.904    230
       2754.76   6.893    215
       2752.56   6.888    701
       2749.63   6.881     72
       2057.98   5.150    132
    

in CDCl3



KBr disc



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