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MassMS-NW-9727 4-bromo-3-nitrobiphenyl C12H8BrNO2 (Mass of molecular ion: 277)
Source Temperature: 210 °C Sample Temperature: 150 °C Reservoir, 75 eV
38.0 1.0 39.0 2.1 50.0 2.9 51.0 4.2 52.0 1.6 55.0 1.7 62.0 3.0 63.0 7.3 67.0 1.1 74.0 3.3 75.0 5.9 75.5 2.3 76.0 12.1 76.5 1.2 77.0 4.1 78.0 4.4 79.0 1.1 87.0 1.3 89.0 1.7 90.0 1.1 94.0 1.6 95.0 1.3 98.0 1.3 99.0 1.4 101.0 1.1 102.0 9.1 103.0 1.0 106.0 2.8 115.0 2.3 121.0 1.0 125.0 1.5 126.0 4.9 127.0 1.4 134.0 5.3 136.0 1.8 139.0 5.6 140.0 6.1 141.0 1.8 146.0 9.0 147.0 6.0 149.0 1.2 150.0 9.3 151.0 17.5 152.0 100.0 153.0 17.6 154.0 1.7 167.0 1.1 168.0 15.6 169.0 2.7 170.0 1.0 181.0 2.7 199.0 6.9 219.0 5.9 221.0 5.9 231.0 5.5 232.0 1.4 233.0 6.3 247.0 2.1 249.0 2.2 277.0 48.1 278.0 6.6 279.0 47.4 280.0 6.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C12 H8 Br N O2 0.034 g : 0.5 ml CDCl3 4-bromo-3-nitrobiphenyl 
Assign. Shift(ppm)
A 8.033 B 7.777 C 7.628 D 7.560 E 7.478 F 7.437
Hz ppm Int.3211.43 8.036 829 3209.23 8.031 837 3113.04 7.790 779 3108.76 7.779 33 3104.61 7.769 1000 3053.47 7.641 585 3051.27 7.635 564 3045.17 7.620 459 3042.97 7.615 444 3027.71 7.576 453 3026.12 7.572 626 3024.05 7.567 196 3021.00 7.560 435 3019.29 7.555 879 3018.07 7.552 780 3015.63 7.546 110 2997.92 7.502 260 2996.22 7.498 346 2994.26 7.493 152 2991.58 7.486 172 2989.99 7.482 603 2989.26 7.480 928 2987.67 7.476 318 2983.28 7.465 297 2981.93 7.462 543 2979.25 7.455 107 2977.91 7.452 283 2976.32 7.448 501 2974.85 7.444 255 2972.05 7.437 151 2969.36 7.430 399 2966.06 7.422 77 2963.38 7.415 74 2962.04 7.412 113 2960.82 7.409 55
in CDCl3
KBr disc
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