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MassMS-NW-9941 4-piperidinopyridine C10H14N2 (Mass of molecular ion: 162)
Source Temperature: 130 °C Sample Temperature: 110 °C Direct, 75 eV
27.0 1.7 28.0 1.8 29.0 1.3 39.0 2.7 41.0 2.8 42.0 1.6 50.0 1.1 51.0 7.5 52.0 2.2 53.0 1.2 55.0 3.0 65.0 1.2 66.0 1.2 67.0 1.1 78.0 11.3 79.0 2.8 80.0 1.0 84.0 1.3 92.0 1.8 93.0 1.2 105.0 11.6 106.0 22.2 107.0 7.0 119.0 2.8 120.0 1.2 121.0 15.6 122.0 1.3 131.0 1.5 132.0 1.7 133.0 8.5 134.0 1.3 145.0 1.0 147.0 3.2 159.0 1.6 160.0 1.6 161.0 100.0 162.0 79.4 163.0 11.5
400 MHz in CDCl3
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1H NMR 399.65 MHz C10 H14 N2 0.035 g : 0.5 ml CDCl3 4-piperidinopyridine 
Assign. Shift(ppm)
A 8.225 B 6.633 C 3.32 D 1.65 to 1.62
Hz ppm Int.3290.53 8.234 263 3284.06 8.218 265 2654.30 6.642 415 2652.71 6.638 292 2649.17 6.629 301 2647.58 6.625 399 1331.18 3.331 321 1326.05 3.319 519 667.60 1.671 30 655.52 1.641 1000 649.17 1.625 198
in CDCl3
KBr disc
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