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MS-NW-5584 cis-9-tricosene C23H46 (Mass of molecular ion: 322)
Source Temperature: 270 °C Sample Temperature: 190 °C Reservoir, 75 eV
18.0 2.3 27.0 8.7 28.0 1.1 29.0 25.7 39.0 6.4 40.0 1.5 41.0 57.4 42.0 11.8 43.0 84.9 44.0 2.9 53.0 4.6 54.0 19.8 55.0 82.1 56.0 45.7 57.0 100.0 58.0 5.3 65.0 1.2 66.0 2.1 67.0 23.8 68.0 17.0 69.0 75.8 70.0 46.8 71.0 52.9 72.0 3.2 77.0 1.2 79.0 3.8 80.0 2.7 81.0 16.9 82.0 28.6 83.0 90.8 84.0 33.4 85.0 33.0 86.0 2.4 93.0 1.2 94.0 1.1 95.0 11.2 96.0 19.6 97.0 81.4 98.0 22.8 99.0 9.9 100.0 1.0 109.0 5.7 110.0 9.0 111.0 43.8 112.0 15.6 113.0 6.3 123.0 3.3 124.0 6.1 125.0 23.2 126.0 10.4 127.0 5.2 137.0 1.8 138.0 4.2 139.0 10.6 140.0 7.1 141.0 3.3 152.0 2.6 153.0 6.6 154.0 5.6 155.0 2.4 166.0 2.0 167.0 4.8 168.0 4.6 169.0 2.0 180.0 1.8 181.0 2.9 182.0 3.3 183.0 1.2 194.0 1.6 195.0 2.2 196.0 2.4 197.0 1.5 208.0 1.1 209.0 1.6 210.0 1.8 211.0 1.1 223.0 1.4 224.0 1.6 237.0 1.2 238.0 1.2 294.0 1.4 320.0 1.8 322.0 11.6 323.0 3.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C23 H46 0.04 ml : 0.5 ml CDCl3 cis-9-tricosene Assign. Shift(ppm)
A 5.35 B 2.01 C 1.26 D 0.88
Hz ppm Int.
478.75 5.346 48 477.50 5.332 23 474.38 5.297 23 183.19 2.046 24 182.88 2.042 25 182.06 2.033 23 177.81 1.986 27 125.69 1.404 22 125.19 1.398 23 123.94 1.384 27 121.56 1.358 35 112.88 1.261 1000 84.06 0.939 40 81.63 0.912 34 81.19 0.907 33 80.75 0.902 33 78.81 0.880 132 72.69 0.812 29
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