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MS-NW-9933 (1-methylcyclopropyl)methanol C5H10O (Mass of molecular ion: 86)
Source Temperature: 190 °C Sample Temperature: 150 °C Reservoir, 75 eV
18.0 1.6 26.0 2.3 27.0 17.0 28.0 8.5 29.0 23.0 30.0 8.8 31.0 14.9 38.0 2.0 39.0 19.8 40.0 7.9 41.0 29.5 42.0 3.2 43.0 13.2 44.0 5.9 45.0 3.1 50.0 2.2 51.0 2.9 52.0 1.0 53.0 11.2 54.0 3.7 55.0 24.1 56.0 46.1 57.0 49.3 58.0 100.0 59.0 4.1 67.0 6.8 68.0 8.8 69.0 2.6 71.0 11.5
400 MHz in CDCl3
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1H NMR 399.65 MHz C5 H10 O 0.05 ml : 0.5 ml CDCl3 (1-methylcyclopropyl)methanol Assign. Shift(ppm)
A 3.367 B 3.02 C 1.141 D *1 0.396 E *1 0.302
Hz ppm Int.
1345.70 3.368 331 1206.67 3.020 201 455.93 1.141 1000 445.56 1.115 25 164.55 0.412 125 160.16 0.401 348 158.57 0.397 384 154.54 0.387 186 125.00 0.313 211 121.09 0.303 405 119.38 0.299 345 114.87 0.288 141
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