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MS-NW-9950 (2-pyridyl)acetonitrile C7H6N2 (Mass of molecular ion: 118)
Source Temperature: 200 °C Sample Temperature: 160 °C Reservoir, 75 eV
26.0 1.7 27.0 2.4 28.0 1.9 37.0 2.2 38.0 3.5 39.0 5.3 40.0 1.6 41.0 1.8 50.0 5.3 51.0 17.7 52.0 5.3 53.0 1.1 61.0 1.1 62.0 2.1 63.0 5.7 64.0 8.7 65.0 3.4 76.0 1.1 78.0 62.5 79.0 3.8 90.0 2.8 91.0 17.9 92.0 2.0 117.0 1.3 118.0 100.0 119.0 8.9
90 MHz in CDCl3
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1H NMR 89.56 MHz C7 H6 N2 0.05 ml : 0.5 ml CDCl3 (2-pyridyl)acetonitrile Assign. Shift(ppm)
A 8.563 B 7.720 C 7.41 D 7.26 E 3.964
Hz ppm Int.
771.00 8.609 109 770.00 8.598 128 769.25 8.590 135 768.31 8.579 125 766.19 8.556 129 765.19 8.544 141 764.38 8.535 142 763.50 8.526 126 701.50 7.833 78 699.69 7.813 77 693.88 7.748 174 692.06 7.728 172 686.25 7.663 175 684.44 7.643 164 666.31 7.440 230 662.75 7.401 39 662.31 7.396 40 661.63 7.388 40 658.31 7.351 159 657.19 7.338 187 655.88 7.324 122 652.31 7.284 129 651.69 7.277 116 651.00 7.269 118 650.38 7.262 105 649.69 7.255 108 649.13 7.248 94 648.44 7.241 91 644.88 7.201 87 644.25 7.194 79 643.56 7.186 77 355.06 3.965 1000
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