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3,5-双三氟甲基苯腈

产品名称 3,5-双三氟甲基苯腈

CAS号27126-93-8

分子式C9H3F6N

分子量239.12

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  • Mass

    MS-NW-9962          
    3,5-bis(trifluoromethyl)benzonitrile
    C9H3F6N             (Mass of molecular ion:    239)
    

       Source Temperature: 240 °C
       Sample Temperature: 160 °C
       Reservoir, 75 eV
    

          28.0       1.2
          31.0       2.7
          38.0       1.1
          50.0       4.6
          51.0       2.0
          57.0       1.9
          69.0      13.3
          74.0       2.8
          75.0      11.2
          76.0       1.6
          87.0       1.4
          88.0       1.1
          93.0       2.0
          94.0       1.0
          99.0       5.8
         100.0       6.4
         101.0       1.5
         119.0       1.7
         120.0       5.0
         123.0       1.0
         124.0       1.6
         125.0       1.1
         139.0       7.1
         143.0       4.6
         144.0       1.5
         150.0       5.9
         151.0       3.3
         163.0       1.4
         168.0       1.2
         169.0       4.1
         170.0      64.3
         171.0       5.9
         188.0       4.7
         189.0      27.2
         190.0       2.5
         213.0       2.0
         219.0       1.8
         220.0      57.5
         221.0       5.9
         238.0       5.6
         239.0     100.0
         240.0      10.1
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C9 H3 F6 N 0.05 ml : 0.5 ml CDCl3
    3,5-bis(trifluoromethyl)benzonitrile
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.173 B 8.151

         Hz     ppm     Int.
    

       3266.72   8.174    970
       3266.24   8.173   1000
       3257.81   8.152    462
    

in CDCl3



liquid film