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MS-NW-8580 N,N-diisopropylformamide C7H15NO (Mass of molecular ion: 129)
Source Temperature: 250 °C Sample Temperature: 130 °C Reservoir, 75 eV
15.0 2.0 18.0 4.3 27.0 7.9 28.0 4.7 29.0 1.5 30.0 1.4 39.0 4.7 41.0 13.8 42.0 9.9 43.0 15.6 44.0 47.0 45.0 1.3 46.0 2.1 58.0 13.8 59.0 1.1 70.0 1.9 72.0 100.0 73.0 3.8 84.0 1.1 86.0 25.0 87.0 1.6 98.0 1.4 100.0 1.5 114.0 18.1 115.0 1.2 129.0 21.0 130.0 5.4
90 MHz in CDCl3
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1H NMR 89.56 MHz C7 H15 N O 0.05 ml : 0.5 ml CDCl3 N,N-diisopropylformamide Assign. Shift(ppm)
A 8.198 B 4.165 C 3.627 D 1.296 E 1.268 ASSIGNED BY C-H AND H-H COSY
Hz ppm Int.
734.25 8.199 143 387.19 4.324 22 380.25 4.246 53 373.44 4.170 71 366.56 4.093 56 359.75 4.017 26 331.88 3.706 44 325.00 3.629 61 318.13 3.553 49 311.44 3.478 22 119.38 1.333 1000 116.88 1.306 878 112.50 1.257 906 110.00 1.229 797 104.06 1.162 25 103.69 1.158 24
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