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网站主页CAS数据库列表 2690-08-6更多图谱1,1’-硫代二辛烷(2690-08-6)核磁图(13CNMR)

1,1’-硫代二辛烷

产品名称 1,1’-硫代二辛烷

CAS号2690-08-6

分子式C16H34S

分子量258.51

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  • Mass

    MS-NW-2737          
    dioctyl sulfide
    C16H34S             (Mass of molecular ion:    258)
    

       Source Temperature: 270 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          27.0       6.2
          28.0       5.1
          29.0      14.9
          32.0       1.3
          39.0       3.7
          41.0      28.1
          42.0       7.6
          43.0      34.4
          44.0       1.1
          45.0       1.7
          46.0       1.1
          47.0       3.3
          53.0       1.5
          54.0       2.0
          55.0      31.8
          56.0      21.8
          57.0      26.0
          58.0       1.3
          60.0       4.5
          61.0      19.6
          62.0       1.0
          63.0       1.0
          67.0       3.3
          68.0       7.4
          69.0      49.5
          70.0      25.9
          71.0      14.9
          75.0       1.8
          81.0       1.5
          82.0       7.2
          83.0      20.7
          84.0      19.3
          85.0       1.8
          87.0       5.6
          88.0       1.0
          89.0       4.4
          97.0       2.5
         101.0       2.6
         103.0       1.3
         111.0       2.5
         112.0      28.6
         113.0       2.7
         144.0       3.8
         145.0     100.0
         146.0      14.1
         147.0       7.1
         159.0      11.0
         160.0       1.5
         173.0       2.8
         201.0       3.4
         229.0       1.1
         257.0       2.4
         258.0      21.1
         259.0       4.1
         260.0       1.4
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C16 H34 S 0.04 ml : 0.5 ml CDCl3
    dioctyl sulfide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.49 B 1.57 C 1.50 to 1.07 D 0.89

         Hz     ppm     Int.
    

        231.19   2.582     91
        230.50   2.574     92
        223.88   2.500    223
        216.56   2.419    193
        148.25   1.656     54
        147.81   1.651     55
        146.81   1.640     52
        146.50   1.636     52
        146.00   1.631     50
        141.19   1.577    122
        140.06   1.564     92
        137.13   1.532     78
        136.31   1.522     79
        134.50   1.502     98
        132.94   1.485     91
        131.50   1.469     95
        131.06   1.464     97
        128.81   1.439    105
        114.31   1.277   1000
        103.56   1.157     39
        103.00   1.151     38
        101.94   1.139     34
         84.19   0.941    138
         81.25   0.908    114
         78.88   0.881    464
         74.44   0.832     64
         72.88   0.814     90
    

in CDCl3



liquid film