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N-(叔丁氧羰基)乙醇胺

产品名称 N-(叔丁氧羰基)乙醇胺

CAS号26690-80-2

分子式C7H15NO3

分子量161.2


  • Mass

    MS-IW-9208          
    tert-butyl (2-hydroxyethyl)carbamate
    C7H15NO3            (Mass of molecular ion:    161)
    

       Source Temperature: 230 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          15.0       2.6
          17.0       3.2
          18.0      16.0
          26.0       1.1
          27.0       7.3
          28.0      12.1
          29.0      19.7
          30.0      65.6
          31.0      10.3
          38.0       1.3
          39.0      12.2
          40.0       3.0
          41.0      53.0
          42.0       6.4
          43.0       6.8
          44.0      20.3
          45.0       3.5
          50.0       1.2
          51.0       1.1
          53.0       1.7
          55.0       6.9
          56.0      16.7
          57.0     100.0
          58.0       5.0
          59.0      47.9
          60.0       3.0
          61.0       2.3
          62.0       5.2
          70.0       3.3
          74.0       1.6
          75.0       3.4
          76.0       8.8
          87.0       1.5
          88.0       9.2
         105.0       4.4
         106.0       3.2
         130.0       5.0
         131.0       4.1
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C7 H15 N O3 0.05 ml : 0.5 ml CDCl3
    tert-butyl (2-hydroxyethyl)carbamate
    ChemicalStructure
        Assign.     Shift(ppm)
    A 5.45 B 3.94 C 3.659 D 3.256 E 1.442

         Hz     ppm     Int.
    

       2178.83   5.452     39
       1467.65   3.673    108
       1462.52   3.660    171
       1457.28   3.647    112
       1304.69   3.265     94
       1299.68   3.253     92
        576.54   1.443   1000
    

in CDCl3



liquid film