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网站主页CAS数据库列表 2651-46-9更多图谱4-氯丁基苯基醚(2651-46-9)核磁图(13CNMR)

4-氯丁基苯基醚

产品名称 4-氯丁基苯基醚

CAS号2651-46-9

分子式C10H13ClO

分子量184.66


  • Mass

    MS-NW-8628          
    4-chlorobutyl phenyl ether
    C10H13ClO           (Mass of molecular ion:    184)
    

       Source Temperature: 260 °C
       Sample Temperature: 140 °C
       Reservoir, 75 eV
    

          27.0       7.9
          28.0       1.5
          29.0       9.8
          38.0       1.5
          39.0      12.8
          40.0       2.4
          41.0       3.4
          49.0       1.3
          50.0       2.2
          51.0       8.2
          53.0       2.5
          55.0      29.7
          56.0       1.3
          63.0       4.1
          64.0       1.1
          65.0      10.2
          66.0      10.7
          77.0      12.4
          78.0       1.2
          79.0       1.6
          91.0      33.2
          92.0       1.7
          93.0      11.1
          94.0     100.0
          95.0       7.0
         107.0       2.4
         184.0       9.1
         185.0       1.0
         186.0       3.0
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C10 H13 Cl O 0.05 ml : 0.5 ml CDCl3
    4-chlorobutyl phenyl ether
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.248 B 6.91 C 6.87 D 3.949 E 3.575 F 2.06 to 1.80 B AND C WERE CONFIRMED BY LAOCN PROGRAM.

         Hz     ppm     Int.
    

        661.44   7.386     42
        659.19   7.361    162
        658.25   7.350    162
        657.31   7.340     96
        656.31   7.329    111
        652.06   7.281    254
        650.69   7.266    442
        648.25   7.239    124
        647.63   7.232    117
        645.19   7.204    220
        643.31   7.184    479
        640.38   7.151     99
        638.31   7.128     37
        627.63   7.008    131
        626.19   6.992    220
        625.13   6.981    236
        621.44   6.939    236
        619.44   6.917   1000
        618.25   6.904    499
        617.50   6.895    498
        615.50   6.873    116
        612.88   6.844    284
        611.75   6.831    279
        610.88   6.821    443
        606.88   6.777     57
        359.69   4.017    224
        358.25   4.001    164
        356.81   3.985    206
        353.81   3.951    632
        352.19   3.933    236
        351.25   3.922    233
        348.06   3.887    234
        346.13   3.865     61
        345.00   3.853     47
        326.63   3.648    194
        324.69   3.626    142
        323.25   3.610    219
        322.38   3.600    234
        320.31   3.577    683
        318.56   3.557    193
        317.31   3.543    199
        315.75   3.526    175
        314.13   3.508    255
        308.63   3.447     31
        187.56   2.095     39
        185.88   2.076     35
        182.81   2.042     85
        179.06   2.000    238
        178.25   1.991    263
        175.13   1.956    599
        172.31   1.924    778
        168.94   1.887    530
        166.06   1.855    290
        162.06   1.810     85
        158.63   1.772     47
        157.56   1.760     46
    

in CDCl3



liquid film



4880 A,200 M,liquid