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MS-NW-1486 L-(-)-alpha-methylbenzylamine C8H11N (Mass of molecular ion: 121)
Source Temperature: 240 °C Sample Temperature: 170 °C Reservoir, 75 eV
15.0 1.3 18.0 2.2 27.0 2.2 28.0 14.2 39.0 3.3 41.0 1.1 42.0 12.2 43.0 6.9 44.0 16.7 50.0 3.6 51.0 8.5 52.0 2.8 53.0 6.2 63.0 1.6 65.0 1.3 74.0 1.2 76.0 1.1 77.0 14.0 78.0 5.3 79.0 24.3 80.0 1.8 91.0 1.3 103.0 3.0 104.0 5.8 105.0 3.8 106.0 100.0 107.0 7.9 120.0 6.1 121.0 1.1
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H11 N 0.04 ml : 0.5 ml CDCl3 L-(-)-alpha-methylbenzylamine Assign. Shift(ppm)
A 7.48 to 7.04 B 4.06 C 1.56 D 1.356
Hz ppm Int.
658.50 7.353 114 656.13 7.327 210 652.69 7.288 786 651.50 7.275 232 650.13 7.260 230 649.13 7.248 97 648.69 7.244 102 647.69 7.232 168 646.56 7.220 98 644.75 7.200 57 644.13 7.193 40 641.69 7.165 51 374.69 4.184 35 368.00 4.109 108 361.44 4.036 116 354.88 3.963 42 139.56 1.559 244 124.81 1.394 1000 118.19 1.320 946
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