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MS-NW-7672 3-nitrobenzylamine hydrochloride C7H8N2O2 HCl (Mass of molecular ion: 152)
Source Temperature: 170 °C Sample Temperature: 140 °C Direct, 75 eV
18.0 1.1 26.0 1.0 27.0 3.7 28.0 25.0 29.0 12.0 30.0 100.0 31.0 1.5 35.0 7.3 36.0 25.9 37.0 2.6 38.0 8.3 39.0 8.9 40.0 1.5 41.0 1.8 46.0 1.2 50.0 14.1 51.0 18.9 52.0 6.8 53.0 2.3 54.0 2.8 61.0 1.2 62.0 3.2 63.0 9.8 64.0 2.6 65.0 2.2 66.0 2.3 67.0 1.6 74.0 4.5 75.0 3.7 76.0 7.5 77.0 48.7 78.0 15.3 79.0 9.3 80.0 1.3 89.0 10.6 90.0 5.4 91.0 2.4 93.0 3.1 94.0 1.7 103.0 1.3 104.0 14.8 105.0 27.9 106.0 18.4 107.0 73.4 108.0 10.2 116.0 1.4 124.0 1.2 125.0 1.4 135.0 1.5 136.0 1.5 151.0 11.1 152.0 2.9
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C7 H8 N2 O2 0.038 g : 0.5 ml DMSO-d6 3-nitrobenzylamine hydrochloride Assign. Shift(ppm)
A 8.87 B 8.500 C 8.238 D 8.053 E 7.734 F 4.209
Hz ppm Int.
3546.75 8.875 370 3397.06 8.501 516 3297.27 8.251 247 3295.75 8.247 232 3289.03 8.230 261 3287.51 8.226 251 3221.74 8.062 284 3213.96 8.042 318 3098.75 7.754 314 3090.82 7.734 498 3082.89 7.714 261 1682.28 4.210 1000
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