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MS-NW-9906 3-chloro-4-fluorophenol C6H4ClFO (Mass of molecular ion: 146)
Source Temperature: 250 °C Sample Temperature: 160 °C Reservoir, 75 eV
31.0 2.6 37.0 1.1 49.0 1.1 50.0 1.4 53.0 1.5 55.0 1.9 56.0 2.6 57.0 8.9 61.0 2.4 62.0 2.1 63.0 6.6 67.0 1.4 73.0 4.8 74.0 2.1 81.0 6.0 82.0 10.7 83.0 39.4 84.0 2.5 91.0 2.4 93.0 1.5 98.0 1.7 110.0 1.5 111.0 2.5 117.0 6.0 118.0 5.4 119.0 2.2 120.0 1.9 126.0 1.0 145.0 1.8 146.0 100.0 147.0 7.2 148.0 32.6 149.0 2.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H4 Cl F O 0.037 g : 0.5 ml CDCl3 3-chloro-4-fluorophenol Assign. Shift(ppm)
A 6.999 B 6.888 C 6.688 D 5.27
Hz ppm Int.
2806.52 7.023 510 2803.10 7.014 26 2797.61 7.001 1000 2794.56 6.993 34 2793.58 6.991 31 2788.94 6.979 584 2785.77 6.971 22 2784.91 6.969 23 2757.45 6.900 541 2754.39 6.893 596 2751.46 6.885 561 2748.41 6.878 582 2680.30 6.707 336 2677.25 6.699 493 2673.58 6.690 325 2671.39 6.685 311 2668.33 6.677 435 2664.67 6.668 275 2106.93 5.272 99
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