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MS-IW-4900 2-chloromethyl-1,3-dioxolane C4H7ClO2 (Mass of molecular ion: 122)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 4.7 19.0 2.8 26.0 1.7 27.0 9.8 28.0 3.6 29.0 10.7 31.0 6.3 36.0 1.1 42.0 3.8 43.0 15.6 44.0 2.1 45.0 33.5 49.0 7.5 50.0 1.6 51.0 2.4 57.0 9.0 61.0 1.0 62.0 1.9 63.0 1.5 73.0 100.0 74.0 4.2 77.0 5.1 79.0 2.1 92.0 4.1 94.0 1.3 121.0 3.3 123.0 1.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C4 H7 Cl O2 0.05 ml : 0.5 ml CDCl3 2-chloromethyl-1,3-dioxolane Assign. Shift(ppm)
A 5.161 B *1 4.049 C *1 3.958 D 3.550
Hz ppm Int.
2066.89 5.172 290 2062.87 5.162 538 2058.84 5.152 282 1634.28 4.090 32 1627.32 4.072 193 1621.95 4.059 292 1620.85 4.056 409 1620.00 4.054 493 1618.16 4.049 342 1616.09 4.044 303 1613.28 4.037 352 1603.76 4.013 151 1596.68 3.996 135 1587.28 3.972 356 1584.47 3.965 293 1582.40 3.960 332 1580.57 3.955 492 1579.71 3.953 349 1578.61 3.950 244 1573.36 3.937 190 1566.28 3.920 39 1420.90 3.556 1000 1416.87 3.546 964
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