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网站主页CAS数据库列表 2567-29-5更多图谱4-溴甲基联苯(2567-29-5)质谱(MS)

4-溴甲基联苯

产品名称 4-溴甲基联苯

CAS号2567-29-5

分子式C13H11Br

分子量247.13

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  • Mass

    MS-IW-9338          
    4-(bromomethyl)biphenyl
    C13H11Br            (Mass of molecular ion:    246)
    

       Source Temperature: 140 °C
       Sample Temperature:  90 °C
       Direct, 75 eV
    

          39.0       1.7
          50.0       1.0
          51.0       1.5
          57.5       1.7
          63.0       2.4
          69.5       2.6
          70.5       2.5
          76.0       1.9
          81.5       1.2
          82.0       5.4
          82.5       7.2
          83.0       4.9
          83.5      11.3
          84.0       1.6
          89.0       1.5
         115.0       2.6
         128.0       1.6
         139.0       2.4
         152.0       6.3
         163.0       1.8
         164.0       2.2
         165.0      17.9
         166.0       5.0
         167.0     100.0
         168.0      15.1
         169.0       1.1
         246.0       5.6
         248.0       5.4
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C13 H11 Br 0.039 g : 0.5 ml CDCl3
    4-(bromomethyl)biphenyl
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.57 B 7.554 C 7.448 D 7.430 E 7.350 F 4.529

         Hz     ppm     Int.
    

       3029.91   7.582    262
       3028.56   7.579    356
       3026.49   7.573    131
       3023.68   7.566    432
       3021.48   7.561    469
       3020.87   7.559    335
       3020.26   7.558    350
       3017.33   7.550    182
       3015.38   7.546    517
       3013.43   7.541     99
       2982.30   7.463    103
       2980.35   7.458    498
       2978.52   7.453    211
       2977.78   7.451    212
       2976.81   7.449    239
       2974.98   7.444    122
       2973.88   7.442    156
       2971.92   7.437    374
       2969.60   7.431    446
       2968.14   7.427    211
       2963.38   7.415    118
       2961.91   7.412    222
       2959.84   7.407     46
       2944.34   7.368     98
       2942.99   7.364    180
       2941.65   7.361    103
       2937.74   7.351     73
       2935.55   7.346    186
       2933.47   7.341     57
       2929.57   7.331     45
       2928.34   7.328     76
       2927.00   7.324     41
       1810.06   4.530   1000
    

in CDCl3



KBr disc



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