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MS-NW-7025 benzyltributylammonium bromide C19H34BrN (Mass of molecular ion: 355)
Source Temperature: 200 °C Sample Temperature: 160 °C Direct, 75 eV
15.0 1.0 17.0 1.1 18.0 4.6 27.0 5.3 28.0 2.8 29.0 16.6 30.0 9.0 38.0 1.9 39.0 7.3 40.0 1.0 41.0 12.8 42.0 8.4 43.0 4.6 44.0 12.2 45.0 1.3 50.0 2.4 51.0 3.1 52.0 1.3 55.0 4.3 56.0 3.0 57.0 10.0 58.0 6.6 62.0 2.1 63.0 4.7 64.0 1.3 65.0 10.8 70.0 1.9 72.0 1.3 84.0 3.6 86.0 3.6 89.0 3.8 90.0 2.2 91.0 76.6 92.0 7.2 98.0 3.8 100.0 33.4 101.0 2.6 128.0 1.2 140.0 1.6 142.0 100.0 143.0 11.3 170.0 4.3 172.0 4.6 176.0 2.5 184.0 1.4 185.0 6.8 186.0 1.1
90 MHz in CDCl3
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1H NMR 89.56 MHz C19 H34 Br N 0.040 g : 0.5 ml CDCl3 benzyltributylammonium bromide Assign. Shift(ppm)
A 7.50 to 7.45 B 4.868 C 3.34 D 1.80 E 1.397 F 0.99
Hz ppm Int.
669.44 7.475 475 440.13 4.915 43 439.69 4.910 49 436.06 4.869 401 432.44 4.829 47 431.63 4.820 32 308.00 3.440 206 300.50 3.356 235 291.50 3.255 294 162.00 1.809 206 123.06 1.375 251 95.19 1.063 626 88.75 0.991 1000 81.38 0.909 264
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