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二乙基硫代磷酰氯

产品名称 二乙基硫代磷酰氯

CAS号2524-04-1

分子式C4H10ClO2PS

分子量188.61

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  • Mass

    MS-NW-2937          
    O,O'-diethyl chlorothiophosphate
    C4H10ClO2PS         (Mass of molecular ion:    188)
    

       Source Temperature: 280 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          14.0       1.4
          15.0       7.3
          26.0       6.6
          27.0      44.1
          28.0      16.0
          29.0      70.4
          30.0       1.5
          31.0       2.0
          32.0       3.9
          34.0       1.6
          35.0       1.6
          36.0       2.4
          42.0       1.3
          43.0      11.9
          44.0       2.7
          45.0      64.7
          46.0       1.9
          47.0      17.9
          48.0       2.4
          58.0       1.3
          59.0       2.2
          60.0       9.0
          61.0       5.2
          62.0       1.4
          63.0       5.9
          64.0       1.1
          65.0      17.7
          67.0       2.2
          79.0       7.2
          80.0       5.0
          81.0       1.0
          83.0      18.3
          85.0       5.6
          91.0       1.7
          93.0       3.5
          96.0       5.1
          97.0      76.3
          98.0       1.9
          99.0       9.8
         100.0       6.0
         101.0       2.2
         102.0       1.8
         108.0       1.5
         110.0       1.2
         111.0      15.9
         113.0       5.3
         114.0       2.0
         115.0      28.9
         116.0      62.2
         117.0      13.1
         118.0      22.2
         119.0       1.6
         121.0       1.9
         125.0      24.8
         126.0       1.7
         127.0       4.2
         128.0       1.5
         129.0       1.5
         131.0       2.4
         132.0      71.5
         133.0      40.7
         134.0      26.7
         135.0      14.8
         136.0       1.3
         143.0       8.7
         144.0      64.7
         145.0       8.2
         146.0      24.2
         147.0       2.0
         148.0       1.1
         153.0      10.8
         159.0       2.2
         160.0       7.7
         161.0      16.1
         162.0       3.3
         163.0       5.5
         188.0     100.0
         189.0       5.9
         190.0      36.1
         191.0       1.9
         192.0       1.5
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C4 H10 Cl O2 P S 0.05 ml : 0.5 ml CDCl3
    O,O'-diethyl chlorothiophosphate
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.300 B 1.414 J(P-31,H(B))=1.0HZ J(P-31,H(A))=11.0HZ

         Hz     ppm     Int.
    

        401.69   4.486     71
        400.56   4.473     77
        394.44   4.405    222
        393.50   4.394    235
        390.69   4.363     87
        390.00   4.355     93
        387.25   4.324    251
        386.50   4.316    249
        383.44   4.282    284
        382.94   4.276    266
        380.13   4.245    107
        379.63   4.239    109
        376.19   4.201    354
        369.13   4.122    173
        133.94   1.496    491
        132.94   1.485    510
        129.13   1.442     30
        126.94   1.418    973
        125.94   1.407   1000
        119.75   1.338    436
        118.81   1.327    445
    

in CDCl3



liquid film





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