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MassMS-NW-4878 O,O'-dimethyl chlorothiophosphate C2H6ClO2PS (Mass of molecular ion: 160)
Source Temperature: 270 °C Sample Temperature: 180 °C Reservoir, 75 eV
14.0 1.9 15.0 28.0 18.0 1.2 28.0 2.9 29.0 8.9 30.0 1.5 31.0 8.0 32.0 2.3 33.0 1.3 36.0 2.1 44.0 1.5 45.0 9.4 46.0 6.5 47.0 54.9 48.0 4.3 49.0 4.0 50.0 11.5 52.0 3.8 61.0 2.1 62.0 5.3 63.0 23.7 64.0 7.0 65.0 1.3 66.0 2.5 67.0 2.5 76.0 1.5 77.0 4.7 79.0 19.7 80.0 2.9 81.0 1.1 83.0 1.6 93.0 13.3 94.0 6.7 95.0 1.9 96.0 1.3 97.0 99.9 98.0 2.9 99.0 33.0 100.0 1.4 110.0 1.2 111.0 1.1 113.0 7.4 114.0 1.9 115.0 4.2 116.0 1.2 125.0 48.6 126.0 2.0 127.0 2.7 129.0 17.1 130.0 92.4 131.0 8.2 132.0 36.0 133.0 1.3 134.0 1.7 141.0 2.0 142.0 1.0 145.0 4.2 146.0 2.1 147.0 1.8 157.0 5.0 160.0 100.0 161.0 3.7 162.0 37.8 163.0 1.3 164.0 1.8 176.0 2.3 180.0 1.9 182.0 1.3 192.0 4.5 194.0 2.1 204.0 1.9
90 MHz in CDCl3
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1H NMR 89.56 MHz C2 H6 Cl O2 P S 0.04 ml : 0.5 ml CDCl3 O,O'-dimethyl chlorothiophosphate 
Assign. Shift(ppm)
A 3.907 J(A,P-31)=16.0HZ
Hz ppm Int.357.88 3.996 1000 356.63 3.983 34 355.56 3.971 23 341.88 3.818 999 340.63 3.804 38
in CDCl3
liquid film
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