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2,6-二氯苯硫酚

产品名称 2,6-二氯苯硫酚

CAS号24966-39-0

分子式C6H4Cl2S

分子量179.07

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  • Mass

    MS-NW-9420          
    2,6-dichlorobenzenethiol
    C6H4Cl2S            (Mass of molecular ion:    178)
    

       Source Temperature: 250 °C
       Sample Temperature: 160 °C
       Reservoir, 75 eV
    

          36.0       2.7
          37.0       3.5
          38.0       2.9
          39.0       2.7
          44.0       1.7
          45.0       5.8
          49.0       2.0
          50.0       2.6
          51.0       1.2
          52.5       1.6
          53.0       7.6
          53.5       1.8
          54.0       1.0
          57.0       1.1
          58.0       2.8
          60.0       1.1
          61.0       4.0
          62.0       5.8
          63.0      13.8
          64.0       1.1
          68.0       1.1
          69.0      17.8
          70.0       1.3
          71.0      10.6
          71.5       1.0
          72.0       4.7
          73.0       7.3
          74.0       6.1
          75.0       5.5
          79.0       3.8
          81.0       6.5
          82.0       6.3
          83.0       1.2
          84.0       2.5
          85.0       1.2
          89.0       5.2
          90.0       4.3
          91.0       1.5
          92.0       1.3
          93.0       1.8
          97.0       2.5
          98.0       1.4
          99.0       4.9
         101.0       1.4
         103.0       2.0
         105.0       2.4
         106.0       3.3
         107.0      34.2
         108.0      19.0
         109.0       5.8
         110.0       1.6
         111.0       1.5
         116.0       1.1
         118.0       2.2
         126.0       1.4
         133.0       2.2
         134.0       5.0
         135.0       1.6
         136.0       3.2
         142.0      40.8
         143.0      73.5
         144.0      20.3
         145.0      28.0
         146.0       4.7
         147.0       1.9
         148.0       1.5
         161.0       5.3
         162.0       3.1
         163.0       3.6
         164.0       1.9
         177.0       4.7
         178.0     100.0
         179.0      10.5
         180.0      68.2
         181.0       5.6
         182.0      13.1
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C6 H4 Cl2 S 0.042 g : 0.5 ml CDCl3
    2,6-dichlorobenzenethiol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.272 B 6.994 C 4.613

         Hz     ppm     Int.
    

        659.69   7.366     68
        657.56   7.343    387
        657.25   7.339    392
        655.88   7.324    434
        655.50   7.320    415
        654.13   7.304     82
        652.38   7.285    106
        649.13   7.248    882
        648.81   7.245    922
        645.38   7.207     79
        635.25   7.094     30
        632.06   7.058    611
        628.94   7.023     31
        628.13   7.014     30
        627.75   7.010     34
        625.31   6.983    378
        624.13   6.969     67
        622.94   6.956    284
        616.25   6.881    201
        413.19   4.614   1000
        410.25   4.581     45
    

in CDCl3



KBr disc



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