-
MassMS-NW-9454 2,2'-methylenediphenol C13H12O2 (Mass of molecular ion: 200)
Source Temperature: 220 °C Sample Temperature: 90 °C Direct, 75 eV
63.0 1.0 76.0 1.8 77.0 4.7 78.0 2.7 79.0 2.2 90.5 1.0 91.0 2.2 94.0 20.4 95.0 1.4 100.0 1.9 106.0 1.5 107.0 100.0 108.0 7.8 115.0 3.8 127.0 1.9 128.0 3.1 131.0 1.6 141.0 1.7 151.0 2.2 152.0 9.5 153.0 6.4 154.0 1.0 165.0 1.7 171.0 1.5 181.0 11.8 182.0 2.4 183.0 1.6 199.0 2.5 200.0 61.7 201.0 8.9
400 MHz in CDCl3
-
1H NMR 399.65 MHz C13 H12 O2 0.031 g : 0.5 ml CDCl3 2,2'-methylenediphenol 
Assign. Shift(ppm)
A 7.635 B 7.273 C 7.058 D 6.882 E 6.800 F 3.925
Hz ppm Int.3051.27 7.635 1000 2911.74 7.286 311 2910.28 7.283 312 2904.17 7.267 344 2902.47 7.263 329 2829.71 7.081 200 2828.00 7.077 200 2825.07 7.069 39 2822.27 7.062 303 2821.78 7.061 299 2820.56 7.058 289 2820.07 7.057 276 2817.26 7.050 30 2816.65 7.048 30 2814.33 7.042 283 2812.62 7.038 257 2757.93 6.901 276 2756.71 6.898 299 2750.49 6.883 455 2749.27 6.880 473 2744.87 6.869 30 2743.04 6.864 227 2741.82 6.861 222 2721.92 6.811 437 2720.83 6.809 395 2713.87 6.791 381 2712.77 6.788 335 1568.85 3.926 773
in CDCl3
KBr disc
nujol mull
更多供应商
