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网站主页CAS数据库列表 2467-02-9更多图谱2,2’-亚甲基双苯酚(2467-02-9)核磁图(1HNMR)

2,2’-亚甲基双苯酚

产品名称 2,2’-亚甲基双苯酚

CAS号2467-02-9

分子式C13H12O2

分子量200.23

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  • Mass

    MS-NW-9454          
    2,2'-methylenediphenol
    C13H12O2            (Mass of molecular ion:    200)
    

       Source Temperature: 220 °C
       Sample Temperature:  90 °C
       Direct, 75 eV
    

          63.0       1.0
          76.0       1.8
          77.0       4.7
          78.0       2.7
          79.0       2.2
          90.5       1.0
          91.0       2.2
          94.0      20.4
          95.0       1.4
         100.0       1.9
         106.0       1.5
         107.0     100.0
         108.0       7.8
         115.0       3.8
         127.0       1.9
         128.0       3.1
         131.0       1.6
         141.0       1.7
         151.0       2.2
         152.0       9.5
         153.0       6.4
         154.0       1.0
         165.0       1.7
         171.0       1.5
         181.0      11.8
         182.0       2.4
         183.0       1.6
         199.0       2.5
         200.0      61.7
         201.0       8.9
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C13 H12 O2 0.031 g : 0.5 ml CDCl3
    2,2'-methylenediphenol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.635 B 7.273 C 7.058 D 6.882 E 6.800 F 3.925

         Hz     ppm     Int.
    

       3051.27   7.635   1000
       2911.74   7.286    311
       2910.28   7.283    312
       2904.17   7.267    344
       2902.47   7.263    329
       2829.71   7.081    200
       2828.00   7.077    200
       2825.07   7.069     39
       2822.27   7.062    303
       2821.78   7.061    299
       2820.56   7.058    289
       2820.07   7.057    276
       2817.26   7.050     30
       2816.65   7.048     30
       2814.33   7.042    283
       2812.62   7.038    257
       2757.93   6.901    276
       2756.71   6.898    299
       2750.49   6.883    455
       2749.27   6.880    473
       2744.87   6.869     30
       2743.04   6.864    227
       2741.82   6.861    222
       2721.92   6.811    437
       2720.83   6.809    395
       2713.87   6.791    381
       2712.77   6.788    335
       1568.85   3.926    773
    

in CDCl3



KBr disc



nujol mull