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MassMS-NW-6124 3,3',3''-(1,2,3-propanetriyltiroxy)tripropionitrile C12H17N3O3 (Mass of molecular ion: 251)
Source Temperature: 230 °C Sample Temperature: 140 °C Direct, 75 eV
15.0 5.0 18.0 1.7 19.0 1.1 26.0 4.5 27.0 11.2 28.0 16.4 29.0 6.5 30.0 1.4 31.0 18.0 39.0 2.2 40.0 1.5 41.0 7.0 42.0 5.3 43.0 11.9 44.0 5.5 45.0 15.5 51.0 1.2 52.0 4.3 53.0 4.4 54.0 100.0 55.0 11.9 56.0 4.2 57.0 10.4 58.0 5.1 59.0 1.0 61.0 3.7 68.0 3.2 69.0 1.7 70.0 1.5 71.0 2.0 72.0 2.5 73.0 7.5 84.0 25.4 85.0 9.7 86.0 13.1 87.0 1.4 96.0 2.4 97.0 19.6 98.0 7.8 107.0 5.5 110.0 12.6 111.0 5.5 112.0 2.5 113.0 17.1 114.0 14.1 115.0 1.0 126.0 2.7 137.0 1.5 139.0 1.2 150.0 1.3 166.0 4.7 167.0 65.0 168.0 6.5 181.0 2.4 182.0 1.9 251.0 1.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C12 H17 N3 O3 0.05 ml : 0.5 ml CDCl3 3,3',3''-(1,2,3-propanetriyltiroxy)tripropionitrile 
Assign. Shift(ppm)
A 3.869 B 3.72 C 3.62 D 2.64
Hz ppm Int.1552.49 3.885 256 1550.29 3.880 33 1546.39 3.870 497 1540.28 3.855 267 1538.09 3.849 35 1501.71 3.758 42 1500.73 3.756 89 1499.39 3.752 37 1495.73 3.743 136 1494.51 3.740 250 1492.19 3.734 304 1490.84 3.731 312 1489.62 3.728 227 1488.40 3.725 284 1486.08 3.719 550 1484.74 3.716 601 1482.18 3.709 186 1479.98 3.704 337 1478.64 3.700 343 1474.98 3.691 112 1472.66 3.685 32 1471.31 3.682 35 1468.99 3.676 36 1465.45 3.667 159 1461.30 3.657 103 1455.20 3.642 358 1451.05 3.631 279 1447.51 3.622 68 1444.82 3.616 350 1438.96 3.601 259 1434.45 3.590 172 1433.23 3.587 108 1430.05 3.579 106 1428.59 3.575 129 1424.32 3.564 85 1420.29 3.554 34 1061.16 2.656 617 1060.42 2.654 415 1055.05 2.640 1000 1054.20 2.638 692 1051.51 2.632 118 1048.95 2.625 541 1048.10 2.623 368
in CDCl3
liquid film
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