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硫化双(苯甲酰甲基)

产品名称 硫化双(苯甲酰甲基)

CAS号2461-80-5

分子式C16H14O2S

分子量270.35

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  • Mass

    MS-NW-8020          
    bis(benzoylmethyl) sulfide
    C16H14O2S           (Mass of molecular ion:    270)
    

       Source Temperature: 180 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          18.0       2.4
          28.0       1.8
          39.0       2.0
          45.0       1.5
          50.0       2.7
          51.0      12.2
          65.0       2.5
          76.0       1.4
          77.0      43.9
          78.0       3.8
          91.0       9.1
         105.0     100.0
         106.0       7.4
         120.0       4.3
         133.0       1.4
         164.0       3.1
         165.0      16.6
         166.0       1.9
         237.0      11.3
         238.0       2.0
         270.0       3.5
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C16 H14 O2 S 0.035 g : 0.5 ml CDCl3
    bis(benzoylmethyl) sulfide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.968 B 7.576 C 7.467 D 3.987

         Hz     ppm     Int.
    

       3191.16   7.985     38
       3189.33   7.981    238
       3188.72   7.979    203
       3187.99   7.977    301
       3187.26   7.976    149
       3186.77   7.974    129
       3186.28   7.973    111
       3182.98   7.965     87
       3180.79   7.959    329
       3179.57   7.956    286
       3037.72   7.601     42
       3036.50   7.598     84
       3035.16   7.595     50
       3031.01   7.585     58
       3029.05   7.580    176
       3027.22   7.575     67
       3022.95   7.564     91
       3021.61   7.561    158
       3020.39   7.558     84
       2993.16   7.490     48
       2991.94   7.487    187
       2991.33   7.485    238
       2989.87   7.482    115
       2984.62   7.469    174
       2983.52   7.466    317
       2982.18   7.462    113
       2977.91   7.452     71
       2976.20   7.448    162
       2975.46   7.446    123
       2974.49   7.443     52
       1593.51   3.988   1000
    

in CDCl3



KBr disc



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