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MassMS-NW-9658 2,3-epoxypropyl 2-ethylhexyl ether C11H22O2 (Mass of molecular ion: 186)
Source Temperature: 260 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 6.2 28.0 6.0 29.0 22.5 30.0 1.2 31.0 19.7 32.0 1.4 39.0 3.7 41.0 28.8 42.0 5.9 43.0 33.5 44.0 1.8 45.0 17.8 53.0 1.4 54.0 1.8 55.0 26.8 56.0 31.3 57.0 100.0 58.0 9.7 59.0 10.2 67.0 1.6 68.0 2.2 69.0 28.5 70.0 32.4 71.0 21.3 72.0 9.5 73.0 2.2 75.0 4.3 81.0 1.6 82.0 3.9 83.0 19.8 84.0 9.9 85.0 2.0 87.0 10.2 97.0 2.6 98.0 5.5 99.0 2.6 111.0 3.6 112.0 9.4 113.0 2.5 129.0 2.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C11 H22 O2 0.05 ml : 0.5 ml CDCl3 2,3-epoxypropyl 2-ethylhexyl ether 
Assign. Shift(ppm)
A *1 3.693 B 3.38 C *1 3.37 D 3.134 E 2.783 F 2.599 G 1.520 J 1.38 to 1.33 K 1.28 L 0.895 M 0.879
Hz ppm Int.1484.50 3.715 102 1483.64 3.713 110 1481.45 3.707 106 1480.47 3.705 109 1472.90 3.686 120 1471.92 3.684 129 1469.85 3.678 124 1468.87 3.676 127 1369.51 3.427 71 1365.97 3.418 65 1363.77 3.413 80 1360.23 3.404 156 1356.57 3.395 237 1354.49 3.390 162 1350.46 3.380 291 1346.80 3.370 153 1344.36 3.364 148 1343.26 3.362 163 1341.06 3.356 160 1338.75 3.350 162 1337.28 3.347 172 1333.98 3.338 75 1331.79 3.333 61 1327.88 3.323 68 1260.25 3.154 61 1257.32 3.147 102 1256.10 3.144 82 1254.52 3.140 121 1253.17 3.136 118 1251.59 3.132 103 1250.37 3.129 129 1248.78 3.125 68 1247.44 3.122 97 1244.63 3.115 55 1116.94 2.795 200 1112.79 2.785 205 1111.82 2.782 249 1107.67 2.772 213 1042.48 2.609 204 1039.79 2.602 203 1037.35 2.596 182 1034.67 2.589 174 612.92 1.534 57 606.93 1.519 83 600.95 1.504 74 594.97 1.489 37 571.78 1.431 32 570.43 1.428 30 565.55 1.416 43 564.33 1.413 60 562.99 1.409 38 558.11 1.397 92 556.76 1.394 89 550.66 1.378 135 549.32 1.375 88 543.33 1.360 165 536.99 1.344 160 536.01 1.342 160 533.94 1.337 70 529.66 1.326 189 526.37 1.318 121 522.34 1.307 223 515.14 1.289 335 512.82 1.284 386 511.35 1.280 384 508.54 1.273 302 506.47 1.268 218 503.91 1.261 117 500.24 1.252 73 497.68 1.246 44 373.66 0.935 33 364.38 0.912 218 363.16 0.909 200 358.76 0.898 646 357.67 0.895 668 351.32 0.880 1000 343.75 0.861 415
in CDCl3
liquid film
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