4-吡咯烷基吡啶

Mass

MS-NW-7651          
4-(1-pyrrolidinyl)pyridine
C9H12N2             (Mass of molecular ion:    148)

   Source Temperature: 250 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      15.0       1.2
      17.0       3.0
      18.0      13.9
      26.0       1.3
      27.0       4.6
      28.0       3.8
      29.0       1.1
      38.0       1.3
      39.0       6.9
      40.0       1.9
      41.0       7.3
      42.0       8.5
      43.0       3.6
      50.0       3.5
      51.0      18.3
      52.0       5.0
      53.0       1.8
      54.0       1.3
      65.0       4.6
      66.0       2.9
      67.0       1.7
      73.0       1.0
      74.0       2.0
      77.0       1.1
      78.0      21.8
      79.0       3.7
      80.0       1.3
      91.0       1.0
      92.0      21.8
      93.0       8.5
      94.0       1.5
     105.0      15.0
     106.0       6.9
     107.0       1.8
     117.0       1.0
     118.0       1.9
     119.0      21.9
     120.0      15.9
     121.0       1.5
     131.0       1.4
     132.0       2.2
     145.0       4.0
     146.0       1.4
     147.0     100.0
     148.0      85.1
     149.0       9.2

Assign. Shift(ppm) A 8.164 B 6.346 C 3.273 D 2.006

     Hz     ppm     Int.

    734.50   8.202    413
    732.94   8.184    315
    729.56   8.147    335
    728.06   8.130    455
    571.56   6.382    483
    570.00   6.365    345
    566.63   6.327    344
    565.06   6.310    457
    300.38   3.354    341
    297.81   3.326    250
    296.13   3.307    315
    293.56   3.278   1000
    291.25   3.253    645
    287.06   3.206    448
    279.38   3.120     34
    278.69   3.112     34
    192.75   2.153     43
    192.00   2.144     41
    186.25   2.080    417
    182.88   2.042    363
    179.63   2.006    966
    176.31   1.969    360
    172.94   1.931    345
    168.19   1.878     43
    167.00   1.865     47